4-溴甲基-3,5-二甲基异噁唑合成路线 (共 3 条)
反应条件
phosphorus tribromide in dichloromethane
T=20°C; 3 h;
参考文献
CHLORION PHARMA, INC.; UNIVERSITE LAVAL; ATTARDO, Giorgio; TRIPATHY, Sasmita
Patent: WO2010/132999 A1, 2010 ;
Location in patent: Page/Page column 109 ;
反应条件
methanol; samarium diiodide in tetrahydrofuran
3 h; Ambient temperature;
参考文献
Natale, Nicholas R.
Tetrahedron Letters, 1982 , vol. 23, # 48 p. 5009 - 5012
反应条件
sodium methylate in methanol
T=0°C;
参考文献
Bravo,P.; Gaviraghi,G.
Journal of Heterocyclic Chemistry, 1977 , vol. 14, p. 37 - 42