hydrogenchloride; acetic acid in water T=120°C; 24 h; Inert atmosphereSealed tube;

1: With aluminum oxide; Wilkinson's catalyst in toluene T=130°C; P=760 Torr; 36 h; Inert atmosphereSealed tube; 2: With hydrogenchloride; acetic acid in water; toluene T=140°C; 48 h;

hydrogenchloride

1: aluminum oxide; Wilkinson's catalyst / 1,4-dioxane / 36 h / 130 °C / 760 Torr / |Inert atmosphere 2: hydrogenchloride; acetic acid / water / 24 h / 120 °C / |Inert atmosphere; |Sealed tube View Scheme

1: Wilkinson's catalyst / 1,4-dioxane / 24 h / 130 °C / 760 Torr / |Inert atmosphere 2: hydrogenchloride; acetic acid / water / 24 h / 120 °C / |Inert atmosphere; |Sealed tube View Scheme