diisobutylaluminium hydride in tetrahydrofuran; dichloromethane T=0°C; 4 h; Inert atmosphere;

borane-THF T=0 - 20°C;

暂无反应条件数据

lithium aluminium tetrahydride in diethyl ether 2 h; Heating;

lithium aluminium tetrahydride

pyridinium chlorochromate in dichloromethane T=20°C; 2 h; Inert atmosphere;

1.1: 14.68 g / imidazole / dimethylformamide / 20 °C 2.1: n-BuLi / tetrahydrofuran; hexane / 0.75 h / -100 °C 2.2: 80 percent / tetrahydrofuran; hexane / 0.75 h / -100 °C 3.1: hydroxylamine hydrochloride / pyridine; ethanol / 60 °C 4.1: 11.85 g / NEt3; DMAP / CH2Cl2 / 0 - 20 °C 5.1: 97 percent / ammonia / diethyl ether / 48 h / 20 °C 6.1: Ag2O / diethyl ether / 1 h / 20 °C 7.1: 5.00 g / TBAF / tetrahydrofuran / 5 h / 0 - 20 °C View Scheme

pyridine in chloroform