in neat (no solvent) 100°C, 5 h; purifn. by severak trap-to-trap distns. to removal OPCl3, then dissoln. in CCl4 and crystn. by adding petroleum ether;
in neat (no solvent) heating with amidosulfuric acid at 100 °C; formation of POCl3 and HCl in the distillate and ClSO2NPCl3 containing only traces of Cl2 as residue;;
参考文献
Kirsanov, A. V.
Zh. obshch. Khim., 1952 , vol. 22, p. 88 - 93
C. A., 1952 , p. 6984
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Gmelin Handbook: P: MVol.C, 192, page 441 - 443
