1: With oxalyl dichloride in dichloromethane 2.5 h; Inert atmosphere; 2: With indium(III) chloride in dichloromethane 3 h; Inert atmosphere;
参考文献
Hylden, Anne T.; Uzelac, Eric J.; Ostojic, Zeljko; Wu, Ting-Ting; Sacry, Keely L.; Sacry, Krista L.; Xi, Lin; Jones, T. Nicholas
Beilstein Journal of Organic Chemistry, 2011 , vol. 7, p. 1323 - 1326
1: hex-5-ynoic acid With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 0.75 h; Inert atmosphere; 2: chloro-trimethyl-silane in tetrahydrofuran; hexane T=-78 - 20°C; Inert atmosphere; 3: With water; acetic acid in tetrahydrofuran; hexane 0.333333 h;
参考文献
Trost, Barry M.; Lehr, Konrad; Michaelis, David J.; Xu, Jiayi; Buckl, Andreas K.
Journal of the American Chemical Society, 2010 , vol. 132, # 26 p. 8915 - 8917
1: hex-5-ynoic acid With oxalyl dichloride in dichloromethane 2.5 h; Inert atmosphere; 2: With indium(III) chloride in dichloromethane 3 h; Inert atmosphere; 3: allyl alcohol in dichloromethane Inert atmosphere;
参考文献
Hylden, Anne T.; Uzelac, Eric J.; Ostojic, Zeljko; Wu, Ting-Ting; Sacry, Keely L.; Sacry, Krista L.; Xi, Lin; Jones, T. Nicholas
Beilstein Journal of Organic Chemistry, 2011 , vol. 7, p. 1323 - 1326
