ammonia in methanol T=180°C; 3 h;

<b>Multi-step reaction with 3 steps<br /> </b>1: 88 percent / dimethylformamide / 1.) r.t., 4 d, 2.) 50 deg C, 8 h<br />2: 78 percent / 1N NaOH / 0.5 h / 100 &deg;C<br />3: 83 percent / 1N NaOH<br /> <br /> &nbsp;