3-甲基-4-氨基苯磺酰胺合成路线 （共 3 条）
反应条件
hydrogenchloride in ethanol; water T=80°C;
参考文献
Sun, Xicheng; Qiu, Jian; Strong, Sarah A.; Green, Louis S.; Wasley, Jan W.F.; Blonder, Joan P.; Colagiovanni, Dorothy B.; Stout, Adam M.; Mutka, Sarah C.; Richards, Jane P.; Rosenthal, Gary J.
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 6 p. 2338 - 2342
反应条件
1: NH4OH / tetrahydrofuran / 0.33 h / 20 °C 2: aq. HCl / ethanol / 1 h / Heating View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 47, # 5 p. 1175 - 1182
反应条件
1.1: pyridine / 2 h / 20 °C 2.1: sodium hydroxide / pyridine / 3 h / 20 °C 2.2: 2 h / -30 - 40 °C 3.1: ammonium hydroxide / tetrahydrofuran / 1 h / 0 - 20 °C 4.1: hydrogenchloride / ethanol; water / 80 °C View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 22, # 6 p. 2338 - 2342
