N-(2-氯苯基)乙酰胺合成路线 (共 129 条)
反应条件
1: Zinc dust, NH4Cl (or NH4Br) 2: NaHCO3 / diethyl ether; H2O / 1 h / T < 5 deg C; or in benzene 3: 82 percent / SOCl2 / diethyl ether / 1 h / T < 5 deg C View Scheme
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 22, # 9 p. 872 - 877
反应条件
1: methanol; acetic acid / Reflux 2: sodium tetrahydroborate; AlCl3, aluminium chloride / tetrahydrofuran / 0 - 50 °C 3: N-(3,4-difluorophenyl)-3-hydroxypropionamide / Irradiation; Neat (no solvent) View Scheme
参考文献
Synthetic Communications, , vol. 42, # 12 p. 1855 - 1863
反应条件
0.266667 h; Microwave irradiationSealed tube; chemoselective reaction;
参考文献
Brahmachari; Laskar; Sarkar
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2010 , vol. 49, # 9 p. 1274 - 1281
反应条件
1: tin; hydrochloric acid View Scheme
参考文献
Zhurnal Russkago Fiziko-Khimicheskago Obshchestva, , vol. 9, p. 101;
Justus Liebigs Annalen der Chemie, , vol. 182, p. 96
反应条件
perchloric acid; toluene
参考文献
Roczniki Chemii, , vol. 32, p. 277,279, 280
Chem.Abstr., , p. 19893
反应条件
K10-montmorillonite in tetrachloromethane T=30°C; Rearrangement; 1 h; Product distribution; Further Variations:TemperaturesReagentstimes;
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 38, # 3 p. 384 - 386
反应条件
T=35°C; P=1 Torr; Rate constant;
参考文献
Journal of the Chemical Society, , p. 953,955
参考文献
Zhurnal Obshchei Khimii, , vol. 3, p. 164,166
Chem. Zentralbl., , vol. 105, # I p. 1476
反应条件
dihydrogen peroxide; nitric acid; sodium chloride in water T=20°C; 1.5 h; influence of the kind of chlorides; efficiency of various acids; Product distribution;
参考文献
Synthetic Communications, , vol. 27, # 18 p. 3291 - 3299
参考文献
Synthetic Communications, , vol. 43, # 18 p. 2508 - 2516