1-叔丁基-4-苯氧基苯合成路线 (共 23 条)
反应条件
[Ni(CH2SiMe3)2(tmen)]; hydrogen; sodium t-butanolate in m-xylene T=120°C; P=750.075 Torr; 48 h; Schlenk technique; regioselective reaction;
参考文献
Journal of the American Chemical Society, , vol. 134, # 50 p. 20226 - 20229
反应条件
copper(l) iodide; caesium carbonate in isobutyl methylketone
T=110°C; Ullmann type condensation; 24 h; Inert atmosphere;
参考文献
Benyahya, Sofia; Monnier, Florian; Wong Chi Man, Michel; Bied, Catherine; Ouazzani, Fouad; Taillefer, Marc
Green Chemistry, 2009 , vol. 11, # 8 p. 1121 - 1123
反应条件
copper(l) iodide; potassium carbonate; Raney Ni-Al alloy in 1,4-dioxane
T=110°C; 16 h;
参考文献
Xu, Li-Wen; Xia, Chun-Gu; Li, Jing-Wei; Hu, Xiao-Xue
Synlett, 2003 , # 13 p. 2071 - 2073
反应条件
caesium carbonate; copper(l) iodide in 1-methyl-pyrrolidin-2-one
T=195°C; 2 h; microwave irradiation;
参考文献
He, Huan; Wu, Yong-Jin
Tetrahedron Letters, 2003 , vol. 44, # 17 p. 3445 - 3446
反应条件
1-methyl-pyrrolidin-2-one
T=120°C; Ullmann diaryl etherification; 5 h; Inert atmosphere;
参考文献
Mulla, Shafeek A.R.; Inamdar, Suleman M.; Pathan, Mohsinkhan Y.; Chavan, Santosh S.
Tetrahedron Letters, 2012 , vol. 53, # 14 p. 1826 - 1829
反应条件
caesium carbonate; copper(l) iodide in 1-methyl-pyrrolidin-2-one
T=195°C; 2 h; microwave irradiation;
参考文献
He, Huan; Wu, Yong-Jin
Tetrahedron Letters, 2003 , vol. 44, # 17 p. 3445 - 3446
反应条件
sodium hydroxide in water
T=20 - 50°C; 6 h;
参考文献
Lindstedt, Erik; Ghosh, Raju; Olofsson, Berit
Organic Letters, 2013 , vol. 15, # 23 p. 6070 - 6073
反应条件
1: phenol With potassium tert-butylate in tetrahydrofuran
T=0°C; 0.25 h;
2: bis(4-tertbutylphenyl)iodonium trifluoromethanesulfonate in tetrahydrofuran
T=40°C; 5 h;
参考文献
Jalalian, Nazli; Petersen, Tue B.; Olofsson, Berit
Chemistry--A European Journal, 2012 , vol. 18, # 44 p. 14140 - 14149,10
反应条件
pyridine; cupric acetate immobilized onto Wang resin in dichloromethane
T=20°C; 24 h;
参考文献
Chiang, Gary C. H.; Olsson, Thomas
Organic Letters, 2004 , vol. 6, # 18 p. 3079 - 3082
反应条件
cesium fluoride in acetonitrile
T=20°C; 24 h;
参考文献
Liu, Zhijian; Larock, Richard C.
Journal of Organic Chemistry, 2006 , vol. 71, # 8 p. 3198 - 3209