1-苯基戊烷-1,3-二酮合成路线 （共 36 条）
反应条件
tin(ll) chloride in dichloromethane
Ambient temperature;
参考文献
Padwa, Albert; Hornbuckle, Susan F.; Zhang, Zhijia; Zhi, Lin
Journal of Organic Chemistry, 1990 , vol. 55, # 18 p. 5297 - 5299
参考文献
Perfetti; Levine
Journal of the American Chemical Society, 1953 , vol. 75, p. 626
反应条件
diethyl ether; sodium amide
Erhitzen des Reaktionsgemisches mit Benzoesaeure-aethylester;
参考文献
Levine et al.
Journal of the American Chemical Society, 1945 , vol. 67, p. 1510
反应条件
sodium hydride in tetrahydrofuran; mineral oil
T=0°C; 16 h; Reflux;
参考文献
Balamurugan, Rengarajan; Manojveer, Seetharaman
Chemical Communications, 2011 , vol. 47, # 39 p. 11143 - 11145
反应条件
diethyl ether; sodium amide
T=-10°C;
参考文献
Michael; Hibbert
Justus Liebigs Annalen der Chemie, 1912 , vol. 390, p. 83
反应条件
1.1: n-butyllithium; diisopropylamine / tetrahydrofuran; hexane / 0.75 h / -78 °C
1.2: -78 °C
2.1: [{(η5-C5Me5)IrCl}2(μ-Cl)2]; SelectF / tetrahydrofuran; water / 1 h / 25 °C
View Scheme
参考文献
Ahlsten, Nanna; Bartoszewicz, Agnieszka; Agrawal, Santosh; Martin-Matute, Belen
Synthesis, 2011 , # 16 art. no. C57411SS, p. 2600 - 2608
反应条件
diethyl ether
Behandeln des Reaktionsgemisches mit Wasser und mit wss. HCl;
参考文献
Mavrodin
Bulet. Soc. Chim. Romania, 1933 , vol. 15, p. 99,102
参考文献
Hoechster Farbw.
Patent: DE43847 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 1, p. 219,597
Full Text Show Details
Stylos
Chemische Berichte, 1887 , vol. 20, p. 2181
反应条件
1.) LSA
1.) THF, -78 deg C, 30 min, 2.) -78 deg C, 20 min; room temp., 40 min; Yield given. Multistep reaction;
参考文献
Sekine, Mitsuo; Kume, Akiko; Nakajima, Masashi; Hata, Tsujiaki
Chemistry Letters, 1981 , p. 1087 - 1090
参考文献
Bogavac,M. et al.
Bulletin de la Societe Chimique de France, 1969 , p. 4437 - 4442
