反应条件
1: 1-benzyl-tetrahydro-thiophenium tetrafluoroborate With lithium hexamethyldisilazane in tetrahydrofuran; dichloromethane
T=-78°C; 1 h;
2: B-allyl-9-BBN in tetrahydrofuran; dichloromethane
T=-100 - 20°C;
3: With sodium hydroxide; dihydrogen peroxide in tetrahydrofuran; dichloromethane
T=20°C; 4 h; Further stages.;
参考文献
Fang, Guang Y.; Wallner, Olov A.; Di Blasio, Nadia; Ginesta, Xavier; Harvey, Jeremy N.; Aggarwal, Varinder K.
Journal of the American Chemical Society, 2007 , vol. 129, # 47 p. 14632 - 14639
