N-溴甲基邻苯二甲酰亚胺合成路线 (共 50 条)
反应条件
phosphorous acid trimethyl ester in anhydrous xylene
参考文献
Besterman, Jeffrey M.; Rahil, Jubrail; Vaisburg, Arkadii
Patent: US2004/29836 A1, 2004 ;
参考文献
Farbenfabr.Bayer
Patent: DE930446 , 1953 ;
反应条件
HCO2Cs in methanol 18 h; RefluxInert atmosphere;
参考文献
Wong, Fung Fuh; Chang, Po-Wei; Lin, Hui-Chang; You, Bang-Jau; Huang, Jiann-Jyh; Lin, Shao-Kai
Journal of Organometallic Chemistry, 2009 , vol. 694, # 21 p. 3452 - 3455
反应条件
in benzene 12 h; Heating; Title compound not separated from byproducts;
参考文献
Coyle, John D.; Newport, Graham L.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 93 - 96
参考文献
Sachs
Chemische Berichte, 1898 , vol. 31, p. 1229
参考文献
Chauhan, Ashok K.S.; Anamika; Kumar, Arun; Srivastava, Ramesh C.; Butcher, Ray J.
Journal of Organometallic Chemistry, 2005 , vol. 690, # 2 p. 313 - 321
参考文献
Vinkler; Szabo
Acta Chimica Academiae Scientiarum Hungaricae, 1951 , vol. 1, p. 103,106
Chem.Abstr., 1952 , p. 2500
反应条件
trimethylsilyl bromide; water; triethyl phosphite 1.) 130-135 deg C, 12 h, 2.) room t., 5 h, 3.) 15 h, reflux; Yield given. Multistep reaction;
参考文献
Chavane
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1947 , vol. 224, p. 406,407
Annales de Chimie (Cachan, France), 1949 , vol. <12>4, p. 377
反应条件
und anschliessend mit wss.Bromwasserstoffsaeure;
参考文献
Chalmers; Kosolapoff
Journal of the American Chemical Society, 1953 , vol. 75, p. 5278
反应条件
1: water 2: phosphorus oxychloride View Scheme
参考文献
Sachs
Chemische Berichte, 1898 , vol. 31, p. 1229