1-(2-(烯丙氧基)苯基)乙酮合成路线 (共 18 条)
反应条件
1: 45 percent / p-TsOH / toluene / 22 h / Heating 2: 12 percent / 650 °C / 0.01 Torr View Scheme
参考文献
Black, Michael; Cadogan; Leardini, Rino; McNab, Hamish; McDougald, Graham; Nanni, Daniele; Reed, David; Zompatori, Alberto
Journal of the Chemical Society - Perkin Transactions 1, 1998 , # 11 p. 1825 - 1832
参考文献
Humne, Vivek; Lokahnde, Pradeep
Synthetic Communications, 2014 , vol. 44, # 7 p. 929 - 935
反应条件
ytterbium(III) triflate in acetonitrile Substitution; Claisen rearrangement; 72 h; Heating;
参考文献
Sharma; Ilangovan; Sreenivas, Punna; Mahalingam
Synlett, 2000 , # 5 p. 615 - 618
反应条件
potassium carbonate; potassium iodide in acetone
Heating;
参考文献
BAYER HEALTHCARE AG
Patent: US2010/35902 A1, 2010 ;
Location in patent: Page/Page column 9; 16 ;
反应条件
potassium iodide; potassium carbonate in acetone; toluene
参考文献
Bayer HealthCare AG
Patent: US2009/214675 A1, 2009 ;
反应条件
copper dichloride in N,N-dimethyl-formamide
1) r.t., 3 h, 2) 50 deg C, 30 min;
参考文献
Ito, Yoshihiko; Nakatsuka, Masashi; Saegusa, Takeo
Journal of Organic Chemistry, 1980 , vol. 45, p. 2022 - 2024
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; n-butyllithium in tetrahydrofuran
T=-78 - 5°C;
参考文献
Nikitin, Kirill V.; Andryukhova, Nonna P.
Canadian Journal of Chemistry, 2004 , vol. 82, # 5 p. 571 - 578
反应条件
sodium hydride in tetrahydrofuran
T=25°C; 80 h;
参考文献
Nikitin, Kirill V.; Andryukhova, Nonna P.
Canadian Journal of Chemistry, 2004 , vol. 82, # 5 p. 571 - 578
反应条件
triphenylphosphine; diethylazodicarboxylate
Mitsunobu allylation;
参考文献
Whitehead, Alan; Moore, Joel D.; Hanson, Paul R.
Tetrahedron Letters, 2003 , vol. 44, # 22 p. 4275 - 4277
反应条件
hydroxy(tosyloxy)iodobenzene in acetonitrile
6 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
De, Surya K.; Mallik, Asok K.
Tetrahedron Letters, 1998 , vol. 39, # 16 p. 2389 - 2390