3-硝基-4-甲基苯乙酮合成路线 （共 17 条）
参考文献
Brady; Day
Journal of the Chemical Society, 1934 , p. 114,119
反应条件
bromine in dichloromethane T=0 - 20°C;
参考文献
PAMLICO PHARMACEUTICAL INC.; ATKINSON, Robert N.; OMMEN, Andy J.; VEAL, James M.; HUANG, Kenneth H.; SMITH, Emilie, D.
Patent: WO2012/88411 A1, 2012 ;
Location in patent: Page/Page column 67 ;
参考文献
Yu; Dingwei Tim; Macina; Orest Taras; Sircar; Ila; Sircar; Jagadish Chandra; Riviello; Christopher Mark
Patent: US6156776 A1, 2000 ;
反应条件
1: tin (II)-chloride; aqueous hydrochloric acid
2: aqueous HCl; acetic acid; concentrated aqueous hydrochloric acid; aqueous CuCl solution
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参考文献
Lutz et al.
Journal of Organic Chemistry, 1947 , vol. 12, p. 617,680
反应条件
1: 2.45 g / SnCl2
2: 1) diazotization 2) boiling 20percent H2SO4
3: 1) Mg / 1) THF 2) a) cooling, 2h b) reflux, 1h
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参考文献
Phadnis, A. P.; Nanda, B.; Patwardhan, Sarita A.; Gupta, A. S.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 11 p. 1098 - 1102
反应条件
1: sodium dithionite; ethanol
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参考文献
Brady; Day
Journal of the Chemical Society, 1934 , p. 114,119
反应条件
1: zinc; aqueous hydrochloric acid
View Scheme
参考文献
Brady; Day
Journal of the Chemical Society, 1934 , p. 114,119
