1,2,3,5-四甲氧基苯合成路线 （共 92 条）
反应条件
sodium; tert-butyl alcohol 3.5 h; Heating;
参考文献
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, , vol. 19, # 5 p. 405 - 406
反应条件
1: AlCl3 2: sodium View Scheme
参考文献
Dhar; Seshadri
Tetrahedron, 1959 , vol. 7, p. 77,80
反应条件
1: aluminum chloride / diethyl ether / 0.5 h / 0 °C 2: aluminum chloride / acetonitrile / 2 h / 50 °C View Scheme
参考文献
Horie, Tokunaru; Tominaga, Hideaki; Kawamura, Yasuhiko; Hada, Takahiko; Ueda, Natsuo; et al.
Journal of Medicinal Chemistry, 1991 , vol. 34, # 7 p. 2169 - 2176
参考文献
Horton; Paul
Journal of Organic Chemistry, 1959 , vol. 24, p. 2000,2002
反应条件
sodium; tert-butyl alcohol 3.5 h; Heating;
参考文献
Sharda, Rekha; Krishnamurty, H. G.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1980 , vol. 19, # 5 p. 405 - 406
反应条件
sodium; tert-butyl alcohol 3 h; Heating; Mechanism;
参考文献
Sharda, Rekha; Krishnamurty, H. G.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1980 , vol. 19, # 5 p. 405 - 406
反应条件
1: AlCl3, aluminium chloride / dichloromethane / 0 - 20 °C / Inert atmosphere 2: potassium carbonate / N,N-dimethyl-formamide / 1.5 h / 60 °C / Inert atmosphere 3: selenium(IV) oxide; dihydrogen peroxide / tert-butyl alcohol / 10 h / 50 °C / Inert atmosphere 4: potassium carbonate / methanol / 3 h / 20 °C / Inert atmosphere 5: potassium carbonate / acetone / 9.5 h / 20 °C / Inert atmosphere 6: AlCl3, aluminium chloride / dichloromethane / 0 - 20 °C 7: lithium hexamethyldisilazane / tetrahydrofuran / -30 - 0 °C / Inert atmosphere 8: trifluoroacetic acid / methanol / 24 h / 50 °C 9: AlCl3, aluminium chloride; ethanethiol / CHCl2 / 0 - 20 °C View Scheme
参考文献
Chemical Communications, , vol. 47, # 10 p. 2868 - 2870
反应条件
1: 3.66 g / AlCl3 / diethyl ether / 1.5 h / 0 °C
2: 2.85 g / AlCl3 / acetonitrile / 1 h / 70 °C
3: 59 percent / aq. NaOH; aq. H2O2 / methanol / 2 h / 3 - 20 °C
4: 7.52 g / K2CO3 / acetone / 1.5 h / 60 °C
5: 75 percent / In(CF3SO3)3 / 0.25 h / microwave irradiation
View Scheme
参考文献
Tsukayama, Masao; Kawamura, Yasuhiko; Ishizuka, Takaaki; Hayashi, Shinji; Torii, Fumihito
Heterocycles, 2003 , vol. 60, # 12 p. 2775 - 2784
反应条件
In(OSO2CF3)3
T=75 - 90°C; 0.1 h; microwave irradiation;
参考文献
Tsukayama, Masao; Kawamura, Yasuhiko; Ishizuka, Takaaki; Hayashi, Shinji; Torii, Fumihito
Heterocycles, 2003 , vol. 60, # 12 p. 2775 - 2784
反应条件
1: AlCl3; diethyl ether
2: sodium acetate
View Scheme
参考文献
Bargellini; Zoras
Gazzetta Chimica Italiana, 1934 , vol. 64, p. 192,197; s.a. E I 732; E II 533
