1,2,3,5-四甲氧基苯合成路线 （共 92 条）
反应条件
carbon disulfide; aluminium trichloride
参考文献
Chapman; Perkin; Robinson
Journal of the Chemical Society, 1927 , p. 3020
Show Details
Bargellini; Bini
Gazzetta Chimica Italiana, 1911 , vol. 41 II, p. 14
Atti della Accademia Nazionale dei Lincei, Classe di Scienze Fisiche, Matematiche e Naturali, Rendiconti, 1910 , vol. <5> 19 II, p. 597
反应条件
aluminium trichloride in diethyl ether
T=22°C; 2 h;
参考文献
Rizzi, George P.
Synthetic Communications, 1983 , vol. 13, # 14 p. 1173 - 1180
反应条件
aluminium trichloride in diethyl ether
T=22°C; 2 h;
参考文献
Rizzi, George P.
Synthetic Communications, 1983 , vol. 13, # 14 p. 1173 - 1180
反应条件
hydrogenchloride; zinc(II) chloride
anschliessende Hydrolyse;
参考文献
Horton; Paul
Journal of Organic Chemistry, 1959 , vol. 24, p. 2000,2002
参考文献
Horton; Paul
Journal of Organic Chemistry, 1959 , vol. 24, p. 2000,2002
反应条件
1: ZnCl2; HCl / anschliessende Hydrolyse
2: HBr; acetic acid
3: sodium acetate; ethanol
4: pyridine
View Scheme
参考文献
Horton; Paul
Journal of Organic Chemistry, 1959 , vol. 24, p. 2000,2002
反应条件
1: 3.66 g / AlCl3 / diethyl ether / 1.5 h / 0 °C
2: 2.85 g / AlCl3 / acetonitrile / 1 h / 70 °C
View Scheme
参考文献
Tsukayama, Masao; Kawamura, Yasuhiko; Ishizuka, Takaaki; Hayashi, Shinji; Torii, Fumihito
Heterocycles, 2003 , vol. 60, # 12 p. 2775 - 2784
反应条件
AlCl3, aluminium chloride in tetrahydrofuran
T=0 - 20°C;
参考文献
Huan Sun, Yi Luan; Schaus, Scott E.
Organic Letters, 2011 , vol. 13, # 24 p. 6480 - 6483
反应条件
aluminium trichloride in diethyl ether
T=30°C; 6 h;
参考文献
Bennett, Graham J.; Lee, Hiok-Huang
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 633 - 638
反应条件
aluminium trichloride in diethyl ether
T=22°C; 17 h; Yield given. Yields of byproduct given;
参考文献
Rizzi, George P.
Synthetic Communications, 1983 , vol. 13, # 14 p. 1173 - 1180
