alpha-(三氯甲基)-4-氯苯甲醇合成路线 (共 32 条)
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene
T=20°C; 12 h;
参考文献
Ram, Ram N.; Manoj
Journal of Organic Chemistry, 2008 , vol. 73, # 14 p. 5633 - 5635
反应条件
malonic acid in dimethyl sulfoxide
T=20°C; 0.666667 h;
参考文献
Jensen, Andreas B.; Lindhardt, Anders T.
Journal of Organic Chemistry, 2014 , vol. 79, # 3 p. 1174 - 1183
反应条件
sodium hydroxide; N-benzyl-N,N,N-triethylammonium chloride in diethyl ether
T=40 - 45°C; 2 h;
参考文献
Volkov, Yu. P.; Yanovskaya, L. A.; Kryshtal', G. V.; Kalinevich, V. M.; Trusova, E. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1986 , vol. 35, # 6 p. 1242 - 1245
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1986 , # 6 p. 1368 - 1372
反应条件
lead(II) bromide; aluminium in N,N-dimethyl-formamide
5 h; Ambient temperature;
参考文献
Tanaka, Hideo; Yamashita, Shiro; Yamanoue, Motoi; Torii, Sigeru
Journal of Organic Chemistry, 1989 , vol. 54, # 2 p. 444 - 450
反应条件
aluminium trichloride
T=-10 - 0°C; 12 h;
参考文献
Menegheli, Paulo; Rezende, Marcos Caroli; Zucco, Cezar
Synthetic Communications, 1987 , vol. 17, # 4 p. 457 - 464
反应条件
lead(II) bromide; aluminium in N,N-dimethyl-formamide
3 h; Ambient temperatureother aldehydes and halomethanes; other metal salts, other solvent, time; Product distribution;
参考文献
Tanaka, Hideo; Yamashita, Shiro; Yamanoue, Motoi; Torii, Sigeru
Journal of Organic Chemistry, 1989 , vol. 54, # 2 p. 444 - 450
参考文献
Sen; Bhargava
Journal of the Indian Chemical Society, 1948 , vol. 25, p. 277,280
Journal of the Indian Chemical Society, 1949 , vol. 26, p. 366
Full Text Show Details
Haller et al.
Journal of the American Chemical Society, 1945 , vol. 67, p. 1591,1599
参考文献
Fry
Journal of the American Chemical Society, 1949 , vol. 71, p. 3238
Full Text Show Details
Barry; Boyer
Canadian Journal of Research, Section B: Chemical Sciences, 1948 , vol. 26, p. 511,515
参考文献
Haller et al.
Journal of the American Chemical Society, 1945 , vol. 67, p. 1591,1599
Full Text Show Details
Gaetzi; Stammbach
Experientia, 1945 , vol. 1, p. 276
Helvetica Chimica Acta, 1946 , vol. 29, p. 563,566
Full Text View citing articles Show Details
Forrest; Stephenson; Waters
Journal of the Chemical Society, 1946 , p. 333,339
反应条件
in N,N-dimethyl-formamide
T=30 - 35°C; 2.33333 h; Product distribution / selectivity;
参考文献
SYNGENTA PARTICIPATIONS AG
Patent: WO2007/20381 A2, 2007 ;
Location in patent: Page/Page column 21 ;