4-氯-1-(4-氯苯基)-1H-吡唑并[3,4-d]嘧啶合成路线 （共 7 条）
反应条件
Mg(2+)*CO4(2-); N-ethyl-N,N-diisopropylamine in tetrahydrofuran
T=200°C; 0.0833333 h; Microwave irradiation;
参考文献
Morrill, Christie; Babu, Suresh; Almstead, Neilg.; Moon, Young-Choon
Synthesis (Germany), 2013 , vol. 45, # 13 art. no. SS-2013-C0248-OP, p. 1791 - 1806
反应条件
in acetonitrile
T=200°C; 0.333333 h; Microwave irradiation;
参考文献
Babu, Suresh; Morrill, Christie; Almstead, Neil G.; Moon, Young-Choon
Organic Letters, 2013 , vol. 15, # 8 p. 1882 - 1885
反应条件
triethylamine in tetrahydrofuran
T=65°C; 1 h;
参考文献
Babu, Suresh; Morrill, Christie; Almstead, Neil G.; Moon, Young-Choon
Organic Letters, 2013 , vol. 15, # 8 p. 1882 - 1885
反应条件
triethylamine in tetrahydrofuran
T=65°C; 1 h; Inert atmosphere; Reagent/catalyst;
参考文献
Morrill, Christie; Babu, Suresh; Almstead, Neilg.; Moon, Young-Choon
Synthesis (Germany), 2013 , vol. 45, # 13 art. no. SS-2013-C0248-OP, p. 1791 - 1806
反应条件
1: triethylamine / tetrahydrofuran / 1 h / 65 °C / |Inert atmosphere
2: acetonitrile / 0.33 h / 200 °C / |Microwave irradiation
View Scheme
参考文献
Morrill, Christie; Babu, Suresh; Almstead, Neilg.; Moon, Young-Choon
Synthesis (Germany), 2013 , vol. 45, # 13 art. no. SS-2013-C0248-OP, p. 1791 - 1806
反应条件
1: triethylamine / tetrahydrofuran / 1 h / 65 °C / |Inert atmosphere
2: acetonitrile / 0.33 h / 200 °C / |Microwave irradiation
View Scheme
参考文献
Morrill, Christie; Babu, Suresh; Almstead, Neilg.; Moon, Young-Choon
Synthesis (Germany), 2013 , vol. 45, # 13 art. no. SS-2013-C0248-OP, p. 1791 - 1806
反应条件
in acetonitrile
T=200°C; 0.0166667 h; Microwave irradiation; TimeConcentration;
参考文献
Morrill, Christie; Babu, Suresh; Almstead, Neilg.; Moon, Young-Choon
Synthesis (Germany), 2013 , vol. 45, # 13 art. no. SS-2013-C0248-OP, p. 1791 - 1806
