3-[N-(苯基)氨基]-3-氧代丙酸乙酯合成路线 （共 19 条）
反应条件
in N,N-dimethyl-formamide 5 h; Heating;
参考文献
Ukrainets, Igor V.; Bezugly, Peter A.; Treskach, Vladimir I.; Taran, Svetlana G.; Gorokhova, Olga V.
Tetrahedron, 1994 , vol. 50, # 34 p. 10331 - 10338
反应条件
ethanol; water; sodium carbonate
参考文献
Chattaway; Olmsted
Journal of the Chemical Society, 1910 , vol. 97, p. 939
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane
T=10 - 20°C; 3 h;
参考文献
KUMIAI CHEMICAL INDUSTRY CO., LTD.; IHARA CHEMICAL INDUSTRY CO., LTD.
Patent: EP1982978 A1, 2008 ;
Location in patent: Page/Page column 82 ;
反应条件
potassium phosphate; tris-(dibenzylideneacetone)dipalladium(0) in toluene
T=60°C; P=760.051 Torr; 6 h;
参考文献
Zhang, Zhenhua; Liu, Yiyang; Ling, Lin; Li, Yuxue; Dong, Yian; Gong, Mingxing; Zhao, Xiaokun; Zhang, Yan; Wang, Jianbo
Journal of the American Chemical Society, 2011 , vol. 133, # 12 p. 4330 - 4341
反应条件
triethylamine in chloroform
T=61°C; 168 h;
参考文献
Nishiwaki, Nagatoshi; Nishida, Daisei; Ohnishi, Tetsuya; Hidaka, Fumie; Shimizu, Satoru; Tamura, Mina; Hori, Kazushige; Tohda, Yasuo; Ariga, Masahiro
Journal of Organic Chemistry, 2003 , vol. 68, # 22 p. 8650 - 8656
反应条件
hydrazine monohydrochloride in ethanol
2 h; Heating;
参考文献
Missio, Lauri J.; Braibante, Hugo S.; Braibante, Mara E. F.
Journal of Heterocyclic Chemistry, 1996 , vol. 33, # 4 p. 1243 - 1245
反应条件
chloro-trimethyl-silane in ethylbenzene
20 h; Reflux;
参考文献
Janikowska, Karolina; Makowiec, Slawomir
Synthetic Communications, 2012 , vol. 42, # 7 p. 975 - 988
反应条件
4-(N,N-dimethlyamino)pyridine; bis-triphenylphosphine-palladium(II) chloride; triethylamine in water; toluene
UV-irradiationAutoclave;
参考文献
Sumino, Shuhei; Fusano, Akira; Fukuyama, Takahide; Ryu, Ilhyong
Synlett, 2012 , vol. 23, # 9 p. 1331 - 1334
反应条件
hydrazine hydrate in ethanol
3 h; Heating;
参考文献
Jung, Jae C.; Watkins, E Blake; Avery, Mitchell A.
Synthetic Communications, 2002 , vol. 32, # 24 p. 3767 - 3777
反应条件
in dichloromethane
T=40°C; 24 h;
参考文献
Nakaike, Yumi; Taba, Noriko; Itoh, Shinobu; Tobe, Yoshito; Nishiwaki, Nagatoshi; Ariga, Masahiro
Bulletin of the Chemical Society of Japan, 2007 , vol. 80, # 12 p. 2413 - 2417
