3-[N-(苯基)氨基]-3-氧代丙酸乙酯合成路线 (共 19 条)
反应条件
tetrabutyl ammonium fluoride; acetic acid
Ambient temperatureIrradiation; Yields of byproduct given;
参考文献
Ang, Kiah H.; Prager, Rolf H.; Williams, Craig M.
Australian Journal of Chemistry, 1995 , vol. 48, # 3 p. 567 - 576
参考文献
Balbi,A. et al.
Farmaco, Edizione Scientifica, 1979 , vol. 34, p. 595 - 611
参考文献
Mahajan, Pankaj S.; Mahajan, Jyoti P.; Mhaske, Santosh B.
Synthetic Communications, 2013 , vol. 43, # 18 p. 2508 - 2516
参考文献
Chattaway; Olmsted
Journal of the Chemical Society, 1910 , vol. 97, p. 939
参考文献
Ruegheimer; Hoffmann
Chemische Berichte, 1884 , vol. 17, p. 236,739
反应条件
1: 59 percent / Na2CO3 / H2O / 4 h
2: 100 percent / toluene-p-sulphonic acid / benzene / 2 h / Heating
View Scheme
参考文献
Lawton, Geoffrey; Moody, Christopher J.; Pearson, Christopher J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 877 - 884
反应条件
1: dimethylformamide / 5 h / Heating
2: 87 percent / 1 h / 155 °C
View Scheme
参考文献
Ukrainets, Igor V.; Bezugly, Peter A.; Treskach, Vladimir I.; Taran, Svetlana G.; Gorokhova, Olga V.
Tetrahedron, 1994 , vol. 50, # 34 p. 10331 - 10338
反应条件
in N,N-dimethyl-formamide
5 h; Heating;
参考文献
Ukrainets, Igor V.; Bezugly, Peter A.; Treskach, Vladimir I.; Taran, Svetlana G.; Gorokhova, Olga V.
Tetrahedron, 1994 , vol. 50, # 34 p. 10331 - 10338
反应条件
in chlorobenzene
20 h; Reflux;
参考文献
Sechi, Mario; Azzena, Ugo; Delussu, Maria Paola; Dallocchio, Roberto; Dessi, Alessandro; Cosseddu, Alessia; Pala, Nicolino; Neamati, Nouri
Molecules, 2008 , vol. 13, # 10 p. 2442 - 2461