2,2 '-二氯-4,4 '-二吡啶合成路线 （共 15 条）
反应条件
1: With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 0.5 h; Inert atmosphere; 2: With iodine in tetrahydrofuran; hexane T=20°C; Inert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 78, # 15 p. 7683 - 7689
反应条件
1: With n-butyllithium in tetrahydrofuran; hexane T=-70°C; Inert atmosphere; 2: With iodine in tetrahydrofuran; hexane T=20°C; Inert atmosphere; Temperature;
参考文献
Journal of Organic Chemistry, , vol. 78, # 15 p. 7683 - 7689
反应条件
1.1: 72 percent / I2; n-BuLi 2.1: 95 percent / LDA 3.1: trimethyltin chloride; n-BuLi 3.2: 53 percent / Pd(PPh3)4 View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 16, # 5 p. 1397 - 1401
反应条件
1.1: 95 percent / LDA 2.1: trimethyltin chloride; n-BuLi 2.2: 53 percent / Pd(PPh3)4 View Scheme
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 16, # 5 p. 1397 - 1401
反应条件
water; sodium carbonate
1 h; Yield given;
参考文献
Brunner, Henri; Stoeriko, Reinhard; Rominger, Frank
European Journal of Inorganic Chemistry, 1998 , # 6 p. 771 - 781
