1,1'-(二硫代二-4,1-亚苯基)二-乙酮合成路线 （共 19 条）
反应条件
chlorine; acetic acid und Behandeln des erhaltenen Sulfonsaeurechlorids mit Ammoniumcarbonat in Chloroform.;
参考文献
Burton; Hu
Journal of the Chemical Society, 1949 , p. 178,179
反应条件
1,10-phenanthroline; CuCl2·2H2O; tetrabutyl ammonium fluoride; caesium carbonate; sulfur in water
T=100°C; 24 h; Sealed tube;
参考文献
Li, Zhengkai; Ke, Fang; Deng, Hang; Xu, Hualong; Xiang, Haifeng; Zhou, Xiangge
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 18 p. 2943 - 2946
反应条件
1,10-phenanthroline; CuCl2·2H2O; tetrabutyl ammonium fluoride; caesium carbonate; sulfur in water
T=100°C; 24 h; Sealed tube;
参考文献
Li, Zhengkai; Ke, Fang; Deng, Hang; Xu, Hualong; Xiang, Haifeng; Zhou, Xiangge
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 18 p. 2943 - 2946
反应条件
tetra-n-butylammonium perchlorate in carbon disulfide; ethanol
T=0°C; Electrochemical reaction;
参考文献
Barba, Fructuoso; Ranz, Fernando; Batanero, Belen
Tetrahedron Letters, 2009 , vol. 50, # 49 p. 6798 - 6799
反应条件
in dimethyl sulfoxide; Petroleum ether
参考文献
Zeneca Limited; Zeneca Pharma S.A.
Patent: US5420298 A1, 1995 ;
US 5420298 A
反应条件
sodium hydroxide
anschliessend mit Jod;
参考文献
Overberger; Lebovits
Journal of the American Chemical Society, 1956 , vol. 78, p. 4792,4795
反应条件
1: NaSMe / dimethylformamide / 1.5 h / 150 °C
2: DFMSO / 18 h / Ambient temperature
View Scheme
参考文献
Crawley, Graham C.; Briggs, Malcolm T.
Journal of Medicinal Chemistry, 1995 , vol. 38, # 20 p. 3951 - 3956
反应条件
1: 92 percent / DMA / 2 h
2: NaSMe / dimethylformamide / 1.5 h / 150 °C
3: DFMSO / 18 h / Ambient temperature
View Scheme
参考文献
Crawley, Graham C.; Briggs, Malcolm T.
Journal of Medicinal Chemistry, 1995 , vol. 38, # 20 p. 3951 - 3956
反应条件
1: AlCl3 / nitrobenzene; CS2
2: H2SO4, AcOH, aq. H2O2
View Scheme
参考文献
Walker,D.
Journal of Organic Chemistry, 1966 , vol. 31, p. 835
反应条件
1: AlCl3 / nitrobenzene; CS2
2: aq. H2O2, H2SO4
View Scheme
参考文献
Walker,D.; Leib,J.
Journal of Organic Chemistry, 1963 , vol. 28, p. 3077 - 3082
