4,4'-二甲氧基二苯二硫合成路线 (共 122 条)
反应条件
dihydrogen peroxide; zirconium tetrachloride in water; acetonitrile T=25°C; 0.0166667 h;
参考文献
Bahrami, Kiumars; Khodaei, Mohammad Mehdi; Soheilizad, Mehdi
Synlett, 2009 , # 17 p. 2773 - 2776
反应条件
hydrogenchloride; diphenylphosphinopolystyrene in tetrahydrofuran 6 h; Heating;
参考文献
Amos, Richard A.; Fawcett, Shayne M.
Journal of Organic Chemistry, 1984 , vol. 49, # 14 p. 2637 - 2639
反应条件
dihydrogen peroxide; methyltrioxorhenium (VII) in acetonitrile T=20°C; 0.166667 h;
参考文献
Ballistreri, Francesco P.; Tomaselli, Gaetano A.; Toscano, Rosa M.
Tetrahedron Letters, 2009 , vol. 50, # 46 p. 6231 - 6232
反应条件
in tetrahydrofuran T=22.4°C; Rate constant;
参考文献
Tagaya, Hideyuki; Aruga, Tamotsu; Ito, Osamu; Matsuda, Minoru
Journal of the American Chemical Society, 1981 , vol. 103, # 18 p. 5484 - 5489
反应条件
thionyl chloride Substitution;
参考文献
Chen, Mark S.; Prabagaran, Narayanasamy; Labenz, Nathan A.; White, M. Christina
Journal of the American Chemical Society, 2005 , vol. 127, # 19 p. 6970 - 6971
反应条件
2,4-di-Nitrobenzene in benzene T=20°C; Addition; 30 h; Irradiation; Further byproducts given. Title compound not separated from byproducts;
参考文献
Leardini, Rino; Nanni, Daniele; Zanardi, Giuseppe
Journal of Organic Chemistry, 2000 , vol. 65, # 9 p. 2763 - 2772
反应条件
1: 1,3-Dichloro-5,5-dimethyl-2,4-imidazolidinedione; water; N-benzyl-N,N,N-trimethyl-ammonium chloride / acetonitrile / 0.5 h / 0 °C 2: ammonia / acetonitrile / 0.5 h / 20 °C View Scheme
参考文献
Veisi, Hojat
Bulletin of the Korean Chemical Society, 2012 , vol. 33, # 2 p. 383 - 386
反应条件
hydrogenchloride in pyridine T=220°C; 0.166667 h;
参考文献
LaLonde, Robert T.; Eckert, Timothy S.
Canadian Journal of Chemistry, 1981 , vol. 59, p. 2298 - 2302
反应条件
1: 1.) LDA / 1.) THF, -70 deg C, 1 h, 2.) THF, -70 deg C, 1 h 2: HCl (conc.) / 2 h / Ambient temperature View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 35, # 2 p. 337 - 345
反应条件
tert.-butylhydroperoxide in benzene T=60°C; Title compound not separated from byproducts;
参考文献
Cole, Edward R.
Phosphorus, Sulfur and Silicon and the Related Elements, 1991 , vol. 63, # 1/2 p. 147 - 160