4,4'-二甲氧基二苯二硫合成路线 （共 122 条）
反应条件
water; 1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate) in acetonitrile
1 h; Reflux;
参考文献
Kirihara, Masayuki; Naito, Sayuri; Nishimura, Yuki; Ishizuka, Yuki; Iwai, Toshiaki; Takeuchi, Haruka; Ogata, Tomomi; Hanai, Honoka; Kinoshita, Yukari; Kishida, Mari; Yamazaki, Kento; Noguchi, Takuya; Yamashoji, Shiro
Tetrahedron, 2014 , vol. 70, # 14 p. 2464 - 2471
反应条件
water; 1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate) in acetonitrile
T=20°C; 0.0166667 h;
参考文献
Kirihara, Masayuki; Naito, Sayuri; Nishimura, Yuki; Ishizuka, Yuki; Iwai, Toshiaki; Takeuchi, Haruka; Ogata, Tomomi; Hanai, Honoka; Kinoshita, Yukari; Kishida, Mari; Yamazaki, Kento; Noguchi, Takuya; Yamashoji, Shiro
Tetrahedron, 2014 , vol. 70, # 14 p. 2464 - 2471
反应条件
tert.-butylhydroperoxide in benzene
T=60°C; Title compound not separated from byproducts;
参考文献
Cole, Edward R.
Phosphorus, Sulfur and Silicon and the Related Elements, 1991 , vol. 63, # 1/2 p. 147 - 160
反应条件
tert.-butylhydroperoxide in benzene
T=60°C; various reaction times; Product distribution;
参考文献
Cole, Edward R.
Phosphorus, Sulfur and Silicon and the Related Elements, 1991 , vol. 63, # 1/2 p. 147 - 160
反应条件
water; 1-(chloromethyl)-4-fluoro-1,4-diazoniabicyclo-[2.2.2]octane bis(tetrafluoroborate) in acetonitrile
T=20°C; 0.0166667 h;
参考文献
Kirihara, Masayuki; Naito, Sayuri; Nishimura, Yuki; Ishizuka, Yuki; Iwai, Toshiaki; Takeuchi, Haruka; Ogata, Tomomi; Hanai, Honoka; Kinoshita, Yukari; Kishida, Mari; Yamazaki, Kento; Noguchi, Takuya; Yamashoji, Shiro
Tetrahedron, 2014 , vol. 70, # 14 p. 2464 - 2471
反应条件
trichloroisocyanuric acid; silica gel
T=20°C; grindingneat (no solvent); chemoselective reaction;
参考文献
Xu, Yali; Peng, Yong; Sun, Junhui; Chen, Jiuxi; Ding, Jinchang; Wu, Huayue
Journal of Chemical Research, 2010 , # 6 p. 358 - 360
反应条件
tert.-butylhydroperoxide in benzene
T=60°C; Title compound not separated from byproducts;
参考文献
Cole, Edward R.
Phosphorus, Sulfur and Silicon and the Related Elements, 1991 , vol. 63, # 1/2 p. 147 - 160
反应条件
tert.-butylhydroperoxide in benzene
T=60°C; various reaction times; Product distribution;
参考文献
Cole, Edward R.
Phosphorus, Sulfur and Silicon and the Related Elements, 1991 , vol. 63, # 1/2 p. 147 - 160
反应条件
iodine in dichloromethane
T=20°C; 3 h;
参考文献
Fujiki, Kiyoko; Tanifuji, Naoki; Sasaki, Yohei; Yokoyama, Taku
Synthesis, 2002 , # 3 p. 343 - 348
反应条件
1: meta-dibromobenzene With bis(η4-1,5-cyclooctadiene)-di-μ-methoxy-diiridium(I); 4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl-4',4',5',5'-tetramethyl-1,3,2-dioxaborolane; 4,4'-di-tert-butyl-2,2'-dipyridyl in tetrahydrofuran
T=80°C; 24 h; Inert atmosphere;
2: bis-(4-methoxyphenyl)-disulfide With [2,2']bipyridinyl; copper(l) chloride in water; dimethyl sulfoxide
T=80°C; 24 h; Inert atmosphere; regioselective reaction;
参考文献
Cheng, Jun-Hao; Yi, Chih-Lun; Liu, Tsung-Jui; Lee, Chin-Fa
Chemical Communications, 2012 , vol. 48, # 67 p. 8440 - 8442
