4,4'-二甲氧基二苯二硫合成路线 (共 122 条)
反应条件
dicobalt octacarbonyl in benzene
T=185°C; P=44080 Torr; in CO-atm.;
参考文献
Antebi, Shlomo; Alper, Howard
Tetrahedron Letters, 1985 , vol. 26, # 22 p. 2609 - 2612
反应条件
1,10-phenanthroline; oxygen; anhydrous copper acetate in dimethyl sulfoxide
T=100°C; 3 h; Air atmosphere;
参考文献
Yasuike, Shuji; Nishioka, Motokazu; Kakusawa, Naoki; Kurita, Jyoji
Tetrahedron Letters, 2011 , vol. 52, # 48 p. 6403 - 6406
反应条件
potassium tert-butylate in dimethyl sulfoxide
T=40 - 80°C;
参考文献
Kumar, Sangit; Kumar, Amit; Bhakuni, Bhagat Singh; Prasad, Ch. Durga; Kumar, Shailesh
Tetrahedron, 2013 , vol. 69, # 26 p. 5383 - 5392
反应条件
[2,2']bipyridinyl; copper(l) iodide in water; dimethyl sulfoxide
T=100°C; 48 h;
参考文献
Taniguchi, Nobukazu
Synlett, 2006 , # 9 p. 1351 - 1354
反应条件
copper(l) iodide; tetrabutyl ammonium fluoride; biphenyl-2-yl-di-tert-butyl-phosphane
T=100°C; 24 h;
参考文献
Luo, Pei-Song; Yu, Ming; Tang, Ri-Yuan; Zhong, Ping; Li, Jin-Heng
Tetrahedron Letters, 2009 , vol. 50, # 9 p. 1066 - 1070
反应条件
tert.-butylhydroperoxide
T=120°C; 18 h; Sealed tubeInert atmosphere;
参考文献
Du, Bingnan; Jin, Bo; Sun, Peipei
Organic Letters, 2014 , vol. 16, # 11 p. 3032 - 3035
反应条件
in toluene
T=20°C; 0.0166667 h; Inert atmosphere;
参考文献
Alvaro, Elsa; Hartwig, John F.
Journal of the American Chemical Society, 2009 , vol. 131, p. 7858 - 7868
反应条件
hydroxymethanesulfinic acid sodium salt; cesium fluoride in water; N,N-dimethyl-formamide
T=20°C; 0.416667 h;
参考文献
Dan, Weixing; Deng, Hongjuan; Chen, Jiuxi; Liu, Miaochang; Ding, Jinchang; Wu, Huayue
Tetrahedron, 2010 , vol. 66, # 37 p. 7384 - 7388
反应条件
ytterbium; methyl iodide in tetrahydrofuran
T=25°C; 1 h;
参考文献
Su, Weike; Li, Yongshu; Zhang, Yongmin
Synthetic Communications, 2002 , vol. 32, # 14 p. 2101 - 2106
反应条件
sulfuryl dichloride in dichloromethane
参考文献
Erashko,V.I. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1974 , vol. 23, p. 1269 - 1273
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1974 , vol. 23, p. 1350 - 1355