4,4'-二甲氧基二苯二硫合成路线 (共 122 条)
反应条件
1: p-methoxyphenyl mercaptan With sulfuryl dichloride; triethylamine in dichloromethane T=0 - 20°C; 2: pyrrolidin-1-yl-2,5-dione With triethylamine in dichloromethane T=0 - 20°C; 1 h;
参考文献
Saravanan, Perumal; Anbarasan, Pazhamalai
Organic Letters, 2014 , vol. 16, # 3 p. 848 - 851
反应条件
CuF2; sulfur in dimethyl sulfoxide T=100°C; Chan-Lam Coupling; 12 h; Inert atmosphere;
参考文献
Yu, Jin-Tao; Guo, Huan; Yi, Yuanqiuqiang; Fei, Haiyang; Jiang, Yan
Advanced Synthesis and Catalysis, 2014 , vol. 356, # 4 p. 749 - 752
反应条件
TPP; oxygen in ethanol; tert-butyl alcohol T=15°C; 0.1 h; Irradiation;
参考文献
Tetrahedron Letters, , vol. 22, # 30 p. 2919 - 2922
反应条件
triethylamine in acetonitrile T=22 - 40°C; 2 h;
参考文献
Journal of Fluorine Chemistry, , vol. 69, # 3 p. 207 - 212
反应条件
tetra-n-butylammonium tetrafluoroborate in acetonitrile T=20°C; Irradiation;
参考文献
Journal of the American Chemical Society, , vol. 117, # 46 p. 11488 - 11498
反应条件
in acetonitrile T=80°C; 22 h; Yields of byproduct given;
参考文献
Tada, Masaru; Kambe, Tohru; Inouye, Yoshinobu
Chemical Communications, 1998 , # 1 p. 41 - 42
反应条件
pyridine; water; benzoic acid in dichloromethane; acetonitrile T=40°C;
参考文献
Zhong; Guo
Synthetic Communications, 2001 , vol. 31, # 12 p. 1825 - 1828
参考文献
Banfield, Scott C.; Omori, Alvaro Takeo; Leisch, Hannes; Hudlicky, Tomas
Journal of Organic Chemistry, 2007 , vol. 72, # 13 p. 4989 - 4992
反应条件
chloro-trimethyl-silane in chloroform 0.5 h; Ambient temperature;
参考文献
Chemistry Letters, , p. 1193 - 1196
反应条件
chloro-trimethyl-silane in chloroform 0.5 h; Ambient temperature;
参考文献
Chemistry Letters, , p. 1193 - 1196