4,4'-二甲氧基二苯二硫合成路线 (共 122 条)
反应条件
antimony(V) pentachloride in dichloromethane T=25°C; 2 h;
参考文献
Takeuchi, Hiroshi; Hiyama, Takehiro; Kamai, Noriyoshi; Oya, Hiromi
Journal of the Chemical Society. Perkin Transactions 2, 1997 , # 11 p. 2301 - 2305
参考文献
Frolov, A. N.; Klokova, E. M.; El'tsov, A. V.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, p. 1926 - 1935
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 10 p. 2161 - 2170
反应条件
N-bromosuccinmide in water; acetonitrile T=20°C; 0.25 h;
参考文献
Kirihara, Masayuki; Naito, Sayuri; Nishimura, Yuki; Ishizuka, Yuki; Iwai, Toshiaki; Takeuchi, Haruka; Ogata, Tomomi; Hanai, Honoka; Kinoshita, Yukari; Kishida, Mari; Yamazaki, Kento; Noguchi, Takuya; Yamashoji, Shiro
Tetrahedron, 2014 , vol. 70, # 14 p. 2464 - 2471
反应条件
sulfuryl dichloride in tetrahydrofuran 1.33333 h; Ambient temperature;
参考文献
Kissei Pharmaceutical Co., Ltd.
Patent: EP1803729 A1, 2007 ;
Location in patent: Page/Page column 65-66 ;
EP 1803729 A1
反应条件
triphenyl methanesulfenyl chloride in chloroform T=20°C; 48 h;
参考文献
Hou, Yihua; Abu-Yousef, Imad A.; Doung, Yen; Harpp, David N.
Tetrahedron Letters, 2001 , vol. 42, # 49 p. 8607 - 8610
反应条件
sulfur; cis-DPPEthylene; [Rh(H)(PEt3)3] in acetone T=20°C; 0.0833333 h;
参考文献
Arisawa, Mieko; Tanaka, Ken; Yamaguchi, Masahiko
Tetrahedron Letters, 2005 , vol. 46, # 28 p. 4797 - 4800
反应条件
tert.-butylhydroperoxide in benzene T=60°C; various reaction times; Product distribution;
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 63, # 1/2 p. 147 - 160
反应条件
hydrogenchloride; zinc in water T=20°C; 0.333333 h; Ionic liquidInert atmosphere;
参考文献
Narayanaperumal, Senthil; Alberto, Eduardo E.; Gul, Kashif; Kawasoko, Cristiane Yuriko; Dornelles, Luciano; Rodrigues, Oscar E.D.; Braga, Antonio Luiz
Tetrahedron, 2011 , vol. 67, # 25 p. 4723 - 4730
反应条件
in tetrahydrofuran T=23°C; Rate constant;
参考文献
Tagaya, Hideyuki; Aruga, Tamotsu; Ito, Osamu; Matsuda, Minoru
Journal of the American Chemical Society, 1981 , vol. 103, # 18 p. 5484 - 5489
反应条件
hydridotetrakis(triphenylphosphine)rhodium (Ph3P)4RhH; 1,2-bis-(diphenylphosphino)ethane in N,N-dimethyl acetamide T=20°C; P=760.051 Torr; 6 h; Inert atmosphere;
参考文献
Arisawa, Mieko; Nihei, Yuri; Yamaguchi, Masahiko
Tetrahedron Letters, 2012 , vol. 53, # 43 p. 5729 - 5732