4-呋喃-2-苯甲酸甲酯合成路线 (共 16 条)
反应条件
lithium chloride; dichlorobis(tris[4-(heptadecafluorooctyl)phenyl]phosphine-kP)palladium in N,N-dimethyl-formamide T=80°C; Stille cross-coupling reaction; 3 h;
参考文献
Angewandte Chemie, International Edition, , vol. 39, # 22 p. 4142 - 4145
Angewandte Chemie, , vol. 112, p. 4293 - 4296
反应条件
chloro porphyrinato gold(III); trifluoroacetic acid in acetone T=60°C; 2 h;
参考文献
Organic Letters, , vol. 8, # 2 p. 325 - 328
反应条件
Pd(OAc)2/XPhos; cesium fluoride in ethylene glycol dimethyl ether T=80°C; Stille coupling; 4 h; Inert atmosphere;
参考文献
Advanced Synthesis and Catalysis, , vol. 350, # 7-8 p. 957 - 961
反应条件
[Ni0(1,5-cyclooctadiene)2]; potassium phosphate; PCy3∙HBF4 in water; tert-butyl alcohol T=110°C; Suzuki-Miyaura cross coupling; 4 h; Inert atmosphere;
参考文献
Organic Letters, , vol. 12, # 18 p. 4022 - 4025
反应条件
palladium diacetate; sodium carbonate; dicyclohexyl(2',6'-diisopropoxy-[1,1'-biphenyl]-2-yl)phosphine in ethanol T=85°C; Suzuki-Miyaura coupling; 8 h; Inert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 74, # 3 p. 973 - 980
参考文献
Journal of Organic Chemistry, , vol. 62, # 21 p. 7295 - 7304
反应条件
tetrakis(triphenylphosphine) palladium(0); N,N-dimethyl acetamide; potassium acetate T=150°C; 12 h;
参考文献
Heterocycles, , vol. 31, # 11 p. 1951 - 1958
反应条件
tetrakis(triphenylphosphine) palladium(0); KF*2H2O in ethylene glycol dimethyl ether; ethanol; water T=110°C; Suzuki Coupling; 0.833333 h; Microwave irradiation;
参考文献
Journal of Medicinal Chemistry, , vol. 56, # 3 p. 761 - 780
反应条件
[Ru(tris(2,2'-bipyridyl))3]Cl2·6H2O in acetonitrile T=25°C; 12 h; Inert atmosphereIrradiationSchlenk technique; regioselective reaction;
参考文献
Synlett, , vol. 24, # 4 art. no. ST-2012-W1056-L, p. 507 - 513
反应条件
1: 2-Furan-2-yl-4,5-dimethyl-[1,3,2]dioxaborolane With 1,1'-bis(diphenylphosphanyl)ferrocenenickel(II) chloride; methyllithium; potassium iodide in tetrahydrofuran T=20°C; 0.25 h; 2: methyl 4-((methylsulfonyl)oxy)benzoate in tetrahydrofuran T=20°C; 14 h;
参考文献
Journal of Organometallic Chemistry, , vol. 653, # 1-2 p. 91 - 97