二甲基-(2-乙烯基-苯基)-胺合成路线 (共 5 条)
反应条件
1: With potassium carbonate in acetonitrile
T=20°C; 1 h;
2: With sodium cyanoborohydride; acetic acid in acetonitrile
T=20°C;
参考文献
Chen, Yan-Yan; Zhang, Xue-Jing; Yuan, Hui-Min; Wei, Wen-Tao; Yan, Ming
Chemical Communications, 2013 , vol. 49, # 93 p. 10974 - 10976
反应条件
tetrabutyl ammonium fluoride; palladium (II) bromide; biphenyl-2-yl-di-tert-butyl-phosphane in tetrahydrofuran
T=50°C; 24 h; Title compound not separated from byproducts;
参考文献
Denmark, Scott E.; Butler, Christopher R.
Organic Letters, 2006 , vol. 8, # 1 p. 63 - 66
反应条件
potassium hydroxide
unter vermindertem Druck;
参考文献
Seeley et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 772
反应条件
2: KOH / unter vermindertem Druck
View Scheme
参考文献
Seeley et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 772
反应条件
water; silver(l) oxide
参考文献
Booth et al.
Journal of the Chemical Society, 1958 , p. 2302,2308