2-氯-1-(1H-吡咯-2-基)-乙酮合成路线 (共 8 条)
反应条件
1: 43 percent / ethanol / 18 h / Heating 2: 15 percent / diethyl ether / 4 h / Irradiation View Scheme
参考文献
Hesabi, Massoud M.; Hill, John; El-Hamamy, Ahmad A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 2371 - 2373
反应条件
zinc oxide in neat (no solvent)
T=20°C; Friedel-Crafts Acylation; 0.05 h; Green chemistry; regioselective reaction;
参考文献
Zhang, Shuguang; Feng, Chengliang; Cai, Jin; Chen, Junqing; Hu, Huayou; Ji, Min
Journal of Chemical Research, 2013 , vol. 37, # 8 p. 480 - 482
反应条件
N,N,N-trimethylbenzenemethanaminium dichloroiodate in tetrahydrofuran
Ambient temperature;
参考文献
Croce, Piero Dalla; Ferraccioli, Rafaella; Ritieni, Alberto
Synthesis, 1990 , # 3 p. 212 - 213
反应条件
hydrogenchloride; diethyl ether
und Erwaermen des Reaktionsprodukts mit Wasser;
参考文献
Knott
Journal of the Chemical Society, 1947 , p. 1656,1658
Full Text Show Details
Blicke et al.
Journal of the American Chemical Society, 1943 , vol. 65, p. 2465
反应条件
diethyl ether
und anschliessend mit wss.Essigsaeure;
参考文献
Blicke et al.
Journal of the American Chemical Society, 1943 , vol. 65, p. 2465
反应条件
trichlorophosphate
1.) room temp., 6 h, 2.) 1,2-dichloroethane, room temp., 16 h; Yield given. Multistep reaction;
参考文献
Croce, Piero Dalla; Rosa, Concetta La; Ritieni, Alberto
Synthesis, 1989 , # 10 p. 783 - 784
参考文献
Oddo; Moschini
Gazzetta Chimica Italiana, 1912 , vol. 42, p. II 260
反应条件
acetone; sodium iodide
参考文献
Blicke et al.
Journal of the American Chemical Society, 1943 , vol. 65, p. 2465