2-甲基-4-戊烯酸乙酯合成路线 （共 13 条）
反应条件
lithium chloride in water; dimethyl sulfoxide 6 h; Heating;
参考文献
Battersby, Alan R.; Westwood, Steven W.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 1679 - 1688
反应条件
propionic acid Heating;
参考文献
Brinkmeyer, Raymond S.; Terando, Norman H.
Journal of Heterocyclic Chemistry, 1989 , vol. 26, p. 1713 - 1717
反应条件
in benzene 1 h; Irradiation;
参考文献
Toru, Takeshi; Yamada, Yoshio; Ueno, Toshio; Maekawa, Eturo; Ueno, Yoshio
Journal of the American Chemical Society, 1988 , vol. 110, # 14 p. 4815 - 4817
反应条件
1.1: NaH / tetrahydrofuran / 0 - 20 °C 1.2: 70 percent / tetrahydrofuran / 4 h / 20 °C 2.1: 65 percent / NaCl / dimethylsulfoxide; H2O / Heating View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 6, # 1 p. 43 - 55
反应条件
1: 97 percent 2: NaH, 1,2-propanediol / tetrahydrofuran / 0.5 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 49, # 4 p. 947 - 964
反应条件
sulfuric acid; benzene
参考文献
Bulletin de la Societe Chimique de France, , p. 634,637
反应条件
pyridine; nickel dichloride; zinc in tetrahydrofuran T=60°C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Wang, Yong; Yang, Zhen-Yu; Burton, Donald J.
Tetrahedron Letters, 1992 , vol. 33, # 16 p. 2137 - 2140
反应条件
n-butyllithium 1) THF-hexane, -78 deg C, 1 h, 2) THF-hexane, -45 deg C, 2 h; Yield givenMultistep reaction;
参考文献
Fleming, Fraser F.; Huang, Adrian; Sharief, Vaqar A.; Pu, Yifang
Journal of Organic Chemistry, 1999 , vol. 64, # 8 p. 2830 - 2834
参考文献
Fleming, Fraser F.; Huang, Adrian; Sharief, Vaqar A.; Pu, Yifang
Journal of Organic Chemistry, 1997 , vol. 62, # 10 p. 3036 - 3037
反应条件
1.1: ozone / dichloromethane / -78 °C 1.2: 18 h / -78 - 20 °C 2.1: 9,10-dimethyl-9,10-dibora-9,10-dihydroanthracene / tetrahydrofuran / 0.08 h 2.2: 16 h / 60 °C View Scheme
参考文献
Kessler, Simon N.; Wegner, Hermann A.
Organic Letters, 2012 , vol. 14, # 13 p. 3268 - 3271
