Alpha-吡啶甲酸正丁酯合成路线 （共 8 条）
反应条件
triethylamine; 1,1'-bis-(diphenylphosphino)ferrocene; bis(benzonitrile)palladium(II) dichloride
T=130°C; P=18751.5 Torr; 15 h;
参考文献
Beller, Matthias; Indolese, Adriano F.
Chimia, 2001 , vol. 55, # 9 p. 684 - 687
反应条件
2,2'-bis-(diphenylphosphino)-1,1'- binaphthyl; triethylamine; palladium dichloride
T=120°C; P=760.051 Torr; 12 h;
参考文献
Yang, Weizhun; Han, Wei; Zhang, Weidong; Shan, Lei; Sun, Jiansong
Synlett, 2011 , # 15 art. no. W10411ST, p. 2253 - 2255
反应条件
copper(l) iodide; 1,10-phenanthroline in o-xylene
T=150°C; 24 h; Inert atmosphere;
参考文献
Nakatani, Yuji; Koizumi, Yuichiro; Yamasaki, Ryu; Saito, Shinichi
Organic Letters, 2008 , vol. 10, # 10 p. 2067 - 2070
反应条件
alumina sulfuric acid
T=110°C; 2 h;
参考文献
Sharghi, Hashem; Sarvari, Mona Hosseini; Eskandari, Razieh
Journal of Chemical Research, 2005 , # 8 p. 488 - 491
参考文献
Williams, R.L.; Neergaard, Sandra
Journal of Heterocyclic Chemistry, 1982 , vol. 19, p. 1549 - 1550
参考文献
Carey et al.
J. econ. Entomol., 1949 , vol. 42, p. 798
反应条件
aluminum oxide
T=200°C; other temperatures, other catalyst; Product distribution;
参考文献
Raja, S.; Xavier, N.; Arulraj, S. J.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1988 , vol. 27, # 1-12 p. 916 - 919
反应条件
1: pyridine-2-carboxylic acid butyl ester With palladium diacetate; 1,2-bis-(diphenylphosphino)ethane in toluene
T=115°C; 0.166667 h;
2: 4-nitrobenzaldehdye With tert.-butylhydroperoxide in toluene
48 h; Reflux;
参考文献
Bao, Yong-Sheng; Chen, Chao-Yue; Huang, Zhi-Zhen
Journal of Organic Chemistry, 2012 , vol. 77, # 18 p. 8344 - 8349,6
