(1R)-(-)-硫代樟脑合成路线 (共 11 条)
反应条件
bis(tricyclohexyltin)sulfide; boron trichloride in toluene 2.5 h; Heating;
参考文献
Steliou,K.; Mrani,M.
Journal of the American Chemical Society, 1982 , vol. 104, p. 3104
反应条件
hydrogen sulfide in benzene T=0 - 5°C; 2 h;
参考文献
Ranise, Angelo; Bondavalli, Francesco; Schenone, Pietro
Journal of Chemical Research, Miniprint, 1984 , # 2 p. 435 - 442
反应条件
disulfur dichloride; triethylamine in benzene T=5°C; 1 h;
参考文献
Okazaki, Renji; Inoue, Kaoru; Inamoto, Naoki
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 11 p. 3541 - 3545
反应条件
(NH4)2S; ethanol T=150°C; Trennung durch Behandeln mit Bleiacetat und Alkohol; thio-d-camphor;
参考文献
Chemische Berichte, , vol. 36, p. 864
反应条件
ammonium hydrosulphide; ethanol thio-d-camphor;
参考文献
Gazzetta Chimica Italiana, , vol. 39 II, p. 206
参考文献
Chemische Berichte, , vol. 39, p. 3505
反应条件
thionyl chloride; dihydrogen peroxide in ethanol T=25°C; 0.0166667 h;
参考文献
Bahrami, Kiumars; Khodaei, Mohammad M.; Farrokhi, Azita
Tetrahedron, 2009 , vol. 65, # 36 p. 7658 - 7661
反应条件
tin(IV) chloride in tert-butyl alcohol T=-78°C; 0.133333 h;
参考文献
Fu, Changchun; Linden, Anthony; Heimgartner, Heinz
Helvetica Chimica Acta, 2003 , vol. 86, # 6 p. 2258 - 2271
反应条件
tin(IV) chloride in dichloromethane T=-78°C; 0.416667 h;
参考文献
Fedorov, Alexey; Fu, Changchun; Heimgartner, Heinz
Helvetica Chimica Acta, 2006 , vol. 89, # 3 p. 456 - 467
反应条件
1: (1R)-(+)-thiocamphor With disulfur dichloride in dichloromethane T=20°C; 0.166667 h; 2: morpholine in dichloromethane T=20°C; 1 h;
参考文献
Tetrahedron, , vol. 68, # 31 p. 6211 - 6217