2-(4-甲氧基苯基)-4,4-二甲基-4,5-二氢-1,3-噁唑合成路线 （共 21 条）
反应条件
thionyl chloride in hydrogenchloride; dichloromethane
参考文献
Zambon Group S.p.A.
Patent: US6329370 B1, 2001 ;
反应条件
1: in chloroform T=80°C; P=206.859 - 517.148 Torr; 0.166667 h; microwave irradiation; 2: With thionyl chloride in chloroform T=80°C; 0.0333333 h; microwave irradiation;
参考文献
Katritzky, Alan R.; Cai, Chunming; Suzuki, Kazuyuki; Singh, Sandeep K.
Journal of Organic Chemistry, 2004 , vol. 69, # 3 p. 811 - 814
反应条件
zinc oxide 0.15 h; microwave irradiation;
参考文献
Garcia-Tellado, Fernando; Loupy, Andre; Petit, Alain; Marrero-Terrero, Alma Leilani
European Journal of Organic Chemistry, 2003 , # 22 p. 4387 - 4391
反应条件
Kaolinitic clay T=165°C; 24 h;
参考文献
Jnaneshwara; Deshpande; Lalithambika; Ravindranathan; Bedekar
Tetrahedron Letters, 1998 , vol. 39, # 5-6 p. 459 - 462
反应条件
C2H3O2(1-)*C20H30OP(1-)*C20H31OP*Pd(2+); lithium tert-butylate in N,N-dimethyl acetamide T=100°C; 14 h; Inert atmosphere;
参考文献
Ackermann, Lutz; Barfuesser, Sebastian; Kornhaass, Christoph; Kapdi, Anant R.
Organic Letters, 2011 , vol. 13, # 12 p. 3082 - 3085
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride in diethyl ether 16 h; Ambient temperature;
参考文献
Pridgen, Lendon N.; Killmer, Lewis B.
Journal of Organic Chemistry, 1981 , vol. 46, # 26 p. 5402 - 5404
反应条件
phosphorus pentoxide in benzene Heating;
参考文献
Sharma, S. D.; Mehra, Usha; Kaur, Sukhjinder
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1984 , vol. 23, # 9 p. 857 - 859
反应条件
1: BuLi / diethyl ether / -78 °C 2: 1) trimethyltin chloride (Me3SnCl) / 2) (Ph3P)4Pd <tetrakis(triphenylphosphine)palladium(O)> / 1) in Et2O, -78 deg C, 2) C6H6, 12h, reflux View Scheme
参考文献
Tetrahedron Letters, , vol. 27, # 43 p. 5269 - 5270
反应条件
1.1: SOCl2 / 0.5 h / 25 °C 1.2: 2 h / 25 °C 2.1: CHCl3 / 0.17 h / 80 °C / 206.86 - 517.15 Torr / microwave irradiation 2.2: 95 percent / SOCl2 / CHCl3 / 0.03 h / 80 °C / microwave irradiation View Scheme
参考文献
Journal of Organic Chemistry, , vol. 69, # 3 p. 811 - 814
反应条件
trimethylstannyl chloride; tetrakis(triphenylphosphine) palladium(0) 1) in Et2O, -78 deg C, 2) C6H6, 12h, reflux; Yield given. Multistep reaction;
参考文献
Tetrahedron Letters, , vol. 27, # 43 p. 5269 - 5270
