4-苯甲酰-4-(2-氰基乙基)庚二腈合成路线 (共 5 条)
参考文献
Campbell; Stevens
Journal of the Chemical Society, 1956 , p. 959,960
反应条件
macroporous anion exchange resin (A-2XMP)
T=20°C; Michael Addition; 1 h; Green chemistry; Catalytic behavior; ConcentrationSolvent; Overall yield = 80 percent; regioselective reaction;
参考文献
Jaitak, Vikas; Kaul; Das, Pralay
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2013 , vol. 52, # 8 p. 1137 - 1145
反应条件
1,4-dioxane; N-benzyl-trimethylammonium hydroxide
参考文献
Bruson; Riener
Journal of the American Chemical Society, 1942 , vol. 64, p. 2857
Journal of the American Chemical Society, 1943 , vol. 65, p. 21
反应条件
1: acetophenone With sodium hydride in toluene
T=0°C; 0.0833333 h;
2: acrylonitrile in toluene
T=0 - 20°C; regioselective reaction;
参考文献
Jaitak, Vikas; Bandna; Das, Pralay; Kaul; Singh, Bikram; Kumar, Neeraj
Synthetic Communications, 2011 , vol. 41, # 18 p. 2727 - 2737
参考文献
Bruson; Riener
Journal of the American Chemical Society, 1942 , vol. 64, p. 2857
Journal of the American Chemical Society, 1943 , vol. 65, p. 21