ethanol in cyclohexane Irradiation (UV/VIS); (Ar); soln. of Ge-compound with ethanol; irradiated with a 110-W low-pressure Hg arc-lamp at room temp. for 1 h; GLC and GC-MS;
参考文献
Journal of Organometallic Chemistry, , vol. 399, # 1/2 p. 53 - 62
tetrachloromethane in cyclohexane byproducts: Me3GeCl; Irradiation (UV/VIS); (Ar); soln. of Ge-compound with CCl4; irradiated with a 110-W low-pressure Hg arc-lamp at room temp. for 1 h; GLC and GC-MS;
参考文献
Journal of Organometallic Chemistry, , vol. 399, # 1/2 p. 53 - 62
tetrachloromethane in cyclohexane byproducts: Me3GeCl; Irradiation (UV/VIS); (Ar); soln. of Ge-compound with CCl4; irradiated with a 110-W low-pressure Hg arc-lamp at room temp. for 1 h; GLC and GC-MS;
参考文献
Journal of Organometallic Chemistry, , vol. 399, # 1/2 p. 53 - 62
in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide
(Ar); soln. of Me3GeCl (2 equiv.) and Ph2GeBr2 (1 equiv.) in THF was added dropwise to soln. of SmI2 (10 equiv.) in THF/hexamethylphosphoric triamide (12/1) for 2 h at room temp.; mixt. was stirred for 1 h; chromd. (silica gel, ether); evapd.; chromd. (silica gel, hexane); elem.anal.;
参考文献
Yokoyama, Yasuo; Hayakawa, Masamichi; Azemi, Takushi; Mochida, Kunio
Journal of the Chemical Society, Chemical Communications, 1995 , # 22 p. 2275 - 2276
