1: diethoxyphosphoryl-acetic acid ethyl ester With sodium hydride in tetrahydrofuran; mineral oil T=0°C; 2: hexadeuterioacetone in tetrahydrofuran; mineral oil T=0 - 20°C; 24 h;

暂无反应条件数据

methanol-d1; diisobutylaluminium hydride in hexane; dichloromethane T=0°C; Reduction; 1.5 h;