3-甲基-2-硝基苯甲醚合成路线 （共 52 条）
反应条件
tert.-butylhydroperoxide; potassium iodide in water; acetonitrile T=80°C; 15 h;
参考文献
Reddy, K. Rajender; Maheswari, C. Uma; Venkateshwar; Kantam, M. Lakshmi
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 1-2 p. 93 - 96
反应条件
potassium carbonate; potassium iodide in acetone Reflux;
参考文献
Yu, Yongguo; Wu, Jianbo; Lei, Fan; Chen, Lei; Wan, Weili; Hai, Li; Guan, Mei; Wu, Yong
Letters in Drug Design and Discovery, 2013 , vol. 10, # 4 p. 369 - 373
反应条件
sodium hydride; dimethyl sulfoxide in tetrahydrofuran T=10 - 20°C; Inert atmosphere;
参考文献
Haiss, Peter; Zeller, Klaus-Peter
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 22 p. 7748 - 7754
反应条件
4-Hydroxy-2-methoxy-6-methylbenzoesaeure-methylester; potassium carbonate; copper(II) oxide T=140°C; 16 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 7 p. 1613 - 1620
反应条件
sodium hydride; dimethyl sulfoxide in tetrahydrofuran T=10 - 20°C; Inert atmosphere;
参考文献
Haiss, Peter; Zeller, Klaus-Peter
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 22 p. 7748 - 7754
反应条件
nitric acid; hydrazine T=25°C; Rate constant;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 94 - 99
反应条件
1: trimethyl-sulfonium iodide With sodium hydride in N,N-dimethyl-formamide; paraffin oil Cooling with iceInert atmosphere; 2: 3-deuterio-2-nitroanisole in N,N-dimethyl-formamide; paraffin oil T=20°C; 16 h; Cooling with iceInert atmosphere;
参考文献
European Journal of Organic Chemistry, , # 2 p. 295 - 301
反应条件
1: trimethyl-sulfonium iodide With sodium hydride in N,N-dimethyl-formamide; paraffin oil Cooling with iceInert atmosphere; 2: o-methoxynitrobenzene in N,N-dimethyl-formamide; paraffin oil T=20°C; 16 h; Cooling with iceInert atmosphere;
参考文献
Haiss, Peter; Zeller, Klaus-Peter
European Journal of Organic Chemistry, 2011 , # 2 p. 295 - 301
反应条件
in dichloromethane T=25°C; 8 h; Irradiation;
参考文献
Sankararaman,S.; Haney,W.A.; Kochi,J.K.
Journal of the American Chemical Society, 1987 , vol. 109, p. 7824
反应条件
1: fuming nitric acid View Scheme
参考文献
Chemische Berichte, , vol. 42, p. 3101
