2,3-二氢-1,5-苯并硫氮杂卓-4(5H)-酮合成路线 （共 24 条）
反应条件
1.1: K2CO3 / dimethylformamide / 20 °C
1.2: 1N aq. NaOH / ethanol / 3 h / 20 °C
2.1: 97 percent / 1N aq. NaOH / methanol / 3 h / 0 °C
View Scheme
参考文献
Wu, Lingyun; Lu, Kai; Desai, Mahesh; Packiarajan, Mathivanan; Joshi, Amita; Marzabadi, Mohammad R.; Jubian, Vrej; Andersen, Kim; Chandrasena, Gamini; Boyle, Noel J.; Walker, Mary W.
Bioorganic and Medicinal Chemistry Letters, 2011 , vol. 21, # 18 p. 5573 - 5576
反应条件
Lawesson's reagent in toluene
T=90 - 100°C; 1.5 h;
参考文献
Ambrogi; Grandolini; Rossi; Tiralti
Farmaco, Edizione Scientifica, 1987 , vol. 42, # 8 p. 575 - 583
反应条件
dihydrogen peroxide; acetic acid
参考文献
Hall
Journal of the American Chemical Society, 1958 , vol. 80, p. 6404,6408
参考文献
Mayer; Horst
Chemische Berichte, 1923 , vol. 56, p. 1423
