5-苄氧基异邻苯二甲酸二甲酯合成路线 （共 6 条）
反应条件
sodium hydroxide in methanol; water 12 h; Reflux;
参考文献
Gole, Bappaditya; Bar, Arun Kumar; Mukherjee, Partha Sarathi
Chemistry - A European Journal, 2014 , vol. 20, # 8 p. 2276 - 2291
反应条件
potassium carbonate in dimethyl sulfoxide; acetone
22 h; Reflux;
参考文献
GLAXO GROUP LIMITED
Patent: WO2004/50619 A1, 2004 ;
Location in patent: Page 29 ;
WO 2004/050619 A1
反应条件
di-isopropyl azodicarboxylate; triphenylphosphine in tetrahydrofuran
T=0 - 25°C; Mitsunobu reaction; Inert atmosphere;
参考文献
Feng, Yu; Liu, Zi-Tong; Liu, Ji; He, Yan-Mei; Zheng, Qi-Yu; Fan, Qing-Hua
Journal of the American Chemical Society, 2009 , vol. 131, p. 7950 - 7951
反应条件
1: 5-hydroxy-isophthalic acid dimethyl ester With potassium carbonate in acetone; acetonitrile
0.5 h; Reflux;
2: benzyl chloride in acetone; acetonitrile
Reflux;
参考文献
Gibson, Harry W.; Wang, Hong; Niu, Zhenbin; Slebodnick, Carla; Zhakharov, Lev N.; Rheingold, Arnold L.
Macromolecules, 2012 , vol. 45, # 3 p. 1270 - 1280
参考文献
Warner-Lambert Company
Patent: US4018825 A1, 1977 ;
反应条件
1: sulfuric acid / 5 h / Reflux
2: potassium carbonate / acetone / 2 h / Reflux
View Scheme
参考文献
Jin, Hao; Xu, Yiding; Shen, Zhihao; Zou, Dechun; Wang, Dan; Zhang, Wei; Fan, Xinghe; Zhou, Qifeng
Macromolecules, 2010 , vol. 43, # 20 p. 8468 - 8478
