5-烯丙基-2-甲氧基-1,3-二甲基苯合成路线 (共 3 条)
反应条件
potassium permanganate
参考文献
Schmid; Schmid
Helvetica Chimica Acta, 1953 , vol. 36, p. 489,496
反应条件
1: T=200°C; 15 h;
2: With sodium hydride in tetrahydrofuran
T=0 - 20°C; 1 h; Inert atmosphere;
3: With methyl iodide in tetrahydrofuran
T=80°C; 15 h; Inert atmosphere;
参考文献
Cardona, Francesca; Isoldi, Giovanni; Sansone, Francesco; Casnati, Alessandro; Goti, Andrea
Journal of Organic Chemistry, 2012 , vol. 77, # 16 p. 6980 - 6988
反应条件
1.1: potassium carbonate / acetone / 15 h / 65 °C
2.1: 15 h / 200 °C
2.2: 1 h / 0 - 20 °C / Inert atmosphere
2.3: 15 h / 80 °C / Inert atmosphere
View Scheme
参考文献
Cardona, Francesca; Isoldi, Giovanni; Sansone, Francesco; Casnati, Alessandro; Goti, Andrea
Journal of Organic Chemistry, 2012 , vol. 77, # 16 p. 6980 - 6988