对甲苯磺酸1-丁炔-3-基酯合成路线 （共 10 条）
参考文献
Lowchol Scientific, Inc.
Patent: US5436273 A1, 1995 ;
反应条件
potassium hydroxide in diethyl ether
参考文献
UNIVERSITE DE MONTREAL
Patent: EP636021 B1, 1998 ;
反应条件
potassium hydroxide in diethyl ether T=-5 - 0°C; 0.5 h;
参考文献
Aidhen; Braslau
Synthetic Communications, 1994 , vol. 24, # 6 p. 789 - 797
参考文献
Larock, R. C.; Varaprath, S.; Lau, H. H.; Fellows, C. A.
Journal of the American Chemical Society, 1984 , vol. 106, # 18 p. 5274 - 5284
反应条件
in N,N-dimethyl-formamide
参考文献
Lowchol Scientific, Inc.
Patent: US5436273 A1, 1995 ;
反应条件
lithium azide; hydrogen; platinum(IV) oxide 1.) CH3OH, 40 deg C, 30 min 2.) RT, 1 d, 1 bar; Yield given. Multistep reaction;
参考文献
Banert, Klaus
Chemische Berichte, 1989 , vol. 122, p. 911 - 918
参考文献
Larock, R. C.; Varaprath, S.; Lau, H. H.; Fellows, C. A.
Journal of the American Chemical Society, 1984 , vol. 106, # 18 p. 5274 - 5284
反应条件
carbon monoxide; triphenylphosphine; bis(dibenzylideneacetone)-palladium(0) in dichloromethane
T=0°C; P=760 Torr; 30 h;
参考文献
Nakamura, Masaki; Yamane, Motoki; Sakurai, Hidehiro; Narasaka, Koichi
Heterocycles, 2003 , vol. 59, # 1 p. 333 - 345
反应条件
sodium hydride in N,N-dimethyl-formamide
6 h; Ambient temperature;
参考文献
Ramana; Sudha
Journal of Mass Spectrometry, 1995 , vol. 30, # 7 p. 1028 - 1033
反应条件
copper(II) bis(trifluoromethanesulfonate) in 1,4-dioxane
T=10 - 20°C; Substitution; 3 h;
参考文献
Wipf, Peter; Hopkins, Corey R.
Journal of Organic Chemistry, 1999 , vol. 64, # 18 p. 6881 - 6887
