N-(4-乙烯基苯基)-乙酰胺合成路线 （共 7 条）
反应条件
caesium carbonate; triphenylphosphine; palladium dichloride in tetrahydrofuran; water
T=85°C; Suzuki-Miyaura reaction; 22 h;
参考文献
Molander, Gary A.; Brown, Adam R.
Journal of Organic Chemistry, 2006 , vol. 71, # 26 p. 9681 - 9686
反应条件
tetrabutyl ammonium fluoride; palladium (II) bromide; biphenyl-2-yl-di-tert-butyl-phosphane in tetrahydrofuran
T=50°C; 12 h;
参考文献
Denmark, Scott E.; Butler, Christopher R.
Organic Letters, 2006 , vol. 8, # 1 p. 63 - 66
反应条件
1: With tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane
T=20°C; 0.25 h; Inert atmosphere;
2: With formic acid in 1,4-dioxane
T=80°C; 3 h; Inert atmosphere;
参考文献
Shen, Ruwei; Chen, Tieqiao; Zhao, Yalei; Qiu, Renhua; Zhou, Yongbo; Yin, Shuangfeng; Wang, Xiangbo; Goto, Midori; Han, Li-Biao
Journal of the American Chemical Society, 2011 , vol. 133, # 42 p. 17037 - 17044
反应条件
pyridine in dichloromethane
Acetylation;
参考文献
Zhuo, Jin-Cong; Wyler, Hugo
Helvetica Chimica Acta, 1999 , vol. 82, # 7 p. 1122 - 1134
反应条件
1: 6.0 g / NH4Cl; Zn powder / H2O; acetone / 0.5 h / Heating
2: 85 percent / pyridine / CH2Cl2
View Scheme
参考文献
Zhuo, Jin-Cong; Wyler, Hugo
Helvetica Chimica Acta, 1999 , vol. 82, # 7 p. 1122 - 1134
反应条件
1: 96 percent / methanesulfonyl chloride; 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 16 h / 0 °C
2: 6.0 g / NH4Cl; Zn powder / H2O; acetone / 0.5 h / Heating
3: 85 percent / pyridine / CH2Cl2
View Scheme
参考文献
Zhuo, Jin-Cong; Wyler, Hugo
Helvetica Chimica Acta, 1999 , vol. 82, # 7 p. 1122 - 1134
参考文献
Komppa
Chemische Berichte, 26 Ref. <1893>,677
Full Text Show Details
Komppa
Dissert. <Helsingfors 1893>, S.44
