(±)-2-乙酰氧基丙酸合成路线 (共 14 条)
反应条件
N-(1-chloro-2-methylprop-1-enyl)-N,N-dimethylamine; copper(l) iodide
1.) THF, dichloromethane, 0 deg C, 3 h; 2.) 0 deg C, 1 h; Yield given. Multistep reaction;
参考文献
Fujisawa, Tamotsu; Mori, Toshiki; Higuchi, Kazunobu; Sato, Toshio
Chemistry Letters, 1983 , p. 1791 - 1794
反应条件
sulfuric acid
T=85°C; P=90 - 110 Torr; in der Dampfphase;
参考文献
Filachione; Fisher
Industrial and Engineering Chemistry, 1944 , vol. 36, p. 473
Full Text Show Details
Filachione
Patent: US2402129 , 1943 ;
反应条件
sulfuric acid
T=140 - 150°C;
参考文献
Filachione; Fisher
Industrial and Engineering Chemistry, 1944 , vol. 36, p. 473
Full Text Show Details
Filachione
Patent: US2402130 , 1943 ;
参考文献
Mattocks,A.R.
Journal of the Chemical Society, 1964 , p. 1918 - 1930