3-(4-甲氧基苯基)-2-硫酮-1,3-噻唑啉-4-酮合成路线 （共 6 条）
反应条件
in water T=95 - 100°C;
参考文献
Liu, Kun; Lu, Hong; Hou, Ling; Qi, Zhi; Teixeira, Catia; Barbault, Florent; Fan, Bo-Tao; Liu, Shuwen; Jiang, Shibo; Xie, Lan
Journal of Medicinal Chemistry, 2008 , vol. 51, # 24 p. 7843 - 7854
反应条件
1: carbon disulfide; 4-methoxy-aniline With sodium hydroxide in water T=100°C; Microwave irradiation; 2: chloroacetic acid in water T=100°C; 0.0833333 h; Microwave irradiation; 3: With hydrogenchloride in water T=120°C; 0.5 h; Microwave irradiation;
参考文献
Nitsche, Christoph; Klein, Christian D.
Tetrahedron Letters, 2012 , vol. 53, # 39 p. 5197 - 5201
反应条件
ammonium hydroxide Erhitzen des Reaktionsprodukts mit Chloressigsaeure-aethylester in Alkohol;
参考文献
Monatshefte fuer Chemie, , vol. 31, p. 894
反应条件
ammonium hydroxide; sodium hydroxide
参考文献
Yakugaku Zasshi, , vol. 79, p. 1462,1464, 1465
Chem.Abstr., , p. 6689
反应条件
(i) aq. Me3N, (ii) Ac2O; Multistep reaction;
参考文献
Journal of the Chemical Society, , p. 3733 - 3735
反应条件
1: aniline With hydrogenchloride; sodium nitrite in water
T=0 - 5°C;
2: 3-(4-methoxyphenyl)-2-thioxo-1,3-thiazolidin-4-one With sodium acetate; potassium hydroxide in ethanol; water
T=0 - 5°C; pH=10 - 12;
参考文献
El-Sonbati; Diab; El-Bindary; Nozha
Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 2011 , vol. 83, # 1 p. 490 - 498
