3-(二乙基氨基)丙酸甲酯合成路线 （共 23 条）
反应条件
hydrogen fluoride T=7 - 8°C; 8.68333 h; electrochemical fluorination;
参考文献
Journal of Fluorine Chemistry, , vol. 57, p. 101 - 111
反应条件
hydrogen fluoride T=7 - 8°C; 8.68333 h; electrochemical fluorination;
参考文献
Abe, Takashi; Hayashi, Eiji; Fukaya, Haruhiko; Hayakawa, Yoshio; Baba, Hajime; et al.
Journal of Fluorine Chemistry, 1992 , vol. 57, p. 101 - 111
反应条件
hydroquinone T=200°C; 8 h; other alkyl 3-(diethylamino)propionates, var. times; also in the presence of diethylamine or methyl acrylate; Product distributionMechanism;
参考文献
Kazantsev, O. A.; Zil'berman, E. N.; Shirshin, K. V.; Krasnov, V. L.; Salov, V. N.
Journal of Organic Chemistry USSR (English Translation), 1991 , vol. 27, # 9.2 p. 1687 - 1691
Zhurnal Organicheskoi Khimii, 1991 , vol. 27, # 9 p. 1914 - 1919
反应条件
hydroquinone T=200°C; 8 h; other alkyl 3-(diethylamino)propionates, var. times; also in the presence of diethylamine or methyl acrylate; Product distributionMechanism;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 27, # 9.2 p. 1687 - 1691
Zhurnal Organicheskoi Khimii, , vol. 27, # 9 p. 1914 - 1919
反应条件
1: hydrazine hydrate / ethanol / 12 h / 20 °C / Reflux 2: hydrogenchloride; sodium nitrate / water / 7 h / 0 - 80 °C View Scheme
参考文献
Asian Journal of Chemistry, , vol. 23, # 9 p. 3792 - 3794
反应条件
methanol; acetic acid; palladium dichloride in carbon dioxide
T=70°C; P=112511 Torr; 48 h; Product distribution; Further Variations:ReagentsPressuresSolvents;
参考文献
Zou, Bo; Jiang, Huan-Feng; Wang, Zhao-Yang
European Journal of Organic Chemistry, 2007 , # 27 p. 4600 - 4604
反应条件
Kuganak montmorillonite
T=20°C; Michael addition; 1.5 h;
参考文献
Dokichev; Latypova; Shakirov; Biglova; Talipov
Russian Journal of Organic Chemistry, 2010 , vol. 46, # 5 p. 755 - 757
反应条件
oxygen; tetrakis(triphenylphosphine) palladium(0) in N,N-dimethyl-formamide
T=75°C; Heck reaction; 24 h;
参考文献
Hosokawa, Takahiro; Kamiike, Taisuke; Murahashi, Shun-Ichi; Shimada, Mamoru; Sugafuji, Toshihiro
Tetrahedron Letters, 2002 , vol. 43, # 51 p. 9323 - 9325
参考文献
Kohjin Co., Ltd.
Patent: US5587515 A1, 1996 ;
反应条件
in dichloromethane
T=25°C; 25 h;
参考文献
Hosomi, Akira; Yanagi, Toshiharu; Hojo, Makoto
Tetrahedron Letters, 1991 , vol. 32, # 21 p. 2371 - 2374
