in methanol; chloroform byproducts: phthalimide-(15)N, (C2H5)3PO; reaction of AuBr3(PEt3) in CHCl3 and K-phthalimide-(15)N in CH3OH;; not separated, detected by NMR-spectroscopy;;

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hydrogenchloride; acetic acid 1) DMF, 90 deg C, 3 h; 12 deg C, 3 d; Yield given. Multistep reaction;

1: N,N-dimethyl-formamide / 12 h / 100 °C / |Inert atmosphere 2: sodium hydroxide; water / 0.5 h / 20 °C 3: hydrogenchloride / water / 12 h / 70 °C View Scheme