1-溴-3-氯-2-丙酮合成路线 (共 13 条)
反应条件
in ethylene glycol dimethyl ether 48 h; Heating;
参考文献
Rival; Grassy; Michel
Chemical and Pharmaceutical Bulletin, 1992 , vol. 40, # 5 p. 1170 - 1176
反应条件
in ethylene glycol dimethyl ether 48 h; Heating;
参考文献
Rival; Grassy; Michel
Chemical and Pharmaceutical Bulletin, 1992 , vol. 40, # 5 p. 1170 - 1176
参考文献
Hanil Pharmaceutical Ind., Co., Ltd.
Patent: US4942243 A1, 1990 ;
反应条件
beim partielle Disproportionierung;
参考文献
Bankowska
Roczniki Chemii, 1959 , vol. 33, p. 1039,1344
Chem.Abstr., 1960 , p. 6525
反应条件
sodium tetrahydroborate in methanol; dichloromethane 0.25 h; Ambient temperature;
参考文献
O'Hagan; White; Jones
Journal of Labelled Compounds and Radiopharmaceuticals, 1994 , vol. 34, # 9 p. 871 - 880
反应条件
beim partielle Disproportionierung;
参考文献
Bankowska
Roczniki Chemii, 1959 , vol. 33, p. 1039,1344
Chem.Abstr., 1960 , p. 6525
反应条件
potassium chloride
T=60 - 80°C; 0.0833333 - 1 h; Product distribution / selectivity;
参考文献
DOW GLOBAL TECHNOLOGIES INC.
Patent: WO2005/115954 A2, 2005 ;
Location in patent: Page/Page column 13-14 ;
反应条件
bromine in 1,4-dioxane; diethyl ether
1 h;
参考文献
Rival; Grassy; Michel
Chemical and Pharmaceutical Bulletin, 1992 , vol. 40, # 5 p. 1170 - 1176
反应条件
hydrogenchloride in diethyl ether
Heating; Yield given;
参考文献
O'Hagan; White; Jones
Journal of Labelled Compounds and Radiopharmaceuticals, 1994 , vol. 34, # 9 p. 871 - 880
反应条件
diethyl ether; water; hydrogen bromide
参考文献
Bankowska
Roczniki Chemii, 1959 , vol. 33, p. 1039,1344
Chem.Abstr., 1960 , p. 6525