1: With diisobutylaluminium hydride in hexane; dichloromethane
T=-78°C; 1.5 h;
2: With hydrogenchloride; water in hexane; dichloromethane
T=-78 - 20°C;
参考文献
Coldham, Iain; Jana, Samaresh; Watson, Luke; Martin, Nathaniel G.
Organic and Biomolecular Chemistry, 2009 , vol. 7, # 8 p. 1674 - 1679
