乙烯基三(三甲基硅氧烷基)硅烷合成路线 (共 11 条)
反应条件
1: bis-trimethylsilyl ether With methanol; sulfuric acid T=5 - 10°C; 1 h; 2: vinyl trimethoxy silane T=5 - 10°C; 1.5 h; 3: With sulfuric acid; water more than 3 stages;
参考文献
Shin-Etsu Chemical Co., Ltd.
Patent: EP1510520 A1, 2005 ;
Location in patent: Page/Page column 12-13 ;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , p. 2022 - 2024
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , p. 2100 - 2102
反应条件
di-isopropyl ether; water
参考文献
Journal of Polymer Science, , vol. 22, p. 55,60
US2851472 , ;
反应条件
in tetrahydrofuran; diethyl ether; pentane 8 h; Heating;
参考文献
Chemische Berichte, , vol. 126, # 10 p. 2177 - 2186
反应条件
T=20°C; Further byproducts given;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 36, # 5 p. 1082 - 1084
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , vol. 36, # 5 p. 1169 - 1171
反应条件
T=20°C; Further byproducts given;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 36, # 5 p. 1082 - 1084
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , vol. 36, # 5 p. 1169 - 1171
反应条件
T=20°C; Further byproducts given;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 36, # 5 p. 1082 - 1084
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , vol. 36, # 5 p. 1169 - 1171
反应条件
[{Ni(η-CH2=CHSiMe2)2O}2{μ-(η-CH2=CHSiMe2)2O}] T=20°C; dehydrogenative coupling; 120 h;
参考文献
Maciejewski; Marciniec; Kownacki
Journal of Organometallic Chemistry, 2000 , vol. 597, # 1-2 p. 175 - 181
反应条件
[{Ni(η-CH2=CHSiMe2)2O}2{μ-(η-CH2=CHSiMe2)2O}] T=120°C; dehydrogenative coupling; 0.5 h;
参考文献
Maciejewski; Marciniec; Kownacki
Journal of Organometallic Chemistry, 2000 , vol. 597, # 1-2 p. 175 - 181
反应条件
[{Ni(η-CH2=CHSiMe2)2O}2{μ-(η-CH2=CHSiMe2)2O}] T=120°C; Addition; dehydrogenative coupling; 24 h;
参考文献
Maciejewski; Marciniec; Kownacki
Journal of Organometallic Chemistry, 2000 , vol. 597, # 1-2 p. 175 - 181